1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE

Base Information

• Chemical Name: 1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE
• CAS No.: 6339-03-3
• Molecular Formula: C30H28 O9
• Molecular Weight: 532.547
• Hs Code.: 2932990090
• Mol file: 6339-03-3.mol

Synonyms:Glucofuranose,1,2-O-isopropylidene-, tribenzoate, a-D- (8CI); Furo[2,3-d]-1,3-dioxole, a-D-glucofuranose deriv.;3,5,6-Tri-O-benzoyl-1,2-O-isopropylidene-a-D-glucofuranose; NSC 38174

Chemical Property of 1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE

Chemical Property:

• Vapor Pressure: 1.31E-16mmHg at 25°C
• Boiling Point: 646.7°C at 760 mmHg
• Flash Point: 273.2°C
• PSA: 106.59000
• Density: 1.34g/cm³
• LogP: 4.17100

Purity/Quality:

1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE

There total 1 articles about 1,2-O-ISOPROPYLIDENE-3,5,6-TRI-O-BENZOYL-ALPHA-D-GLUCOFURANOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ O3,O5,O6-tribenzoyl-O1,O2-isopropylidene-α-D-glucofuranose (6339-03-3)

Guidance literature:

Reference yield: 70.0%

O3,O5,O6-tribenzoyl-O1,O2-isopropylidene-α-D-glucofuranose (6339-03-3) + ethanethiol (75-08-1) → O4,O5,O6-tribenzoyl-S2,S3-diethyl-D-2,3-dithio-allose diethyl dithioacetal (35919-95-0)

Guidance literature:

With hydrogenchloride; 1) 0 deg C, 3 h, 2) RT, 20 h;

DOI:10.1016/S0008-6215(00)90940-6

Reference yield:

O3,O5,O6-tribenzoyl-O1,O2-isopropylidene-α-D-glucofuranose (6339-03-3) + ethanethiol (75-08-1) → D-glucose diethyl mercaptal (1941-52-2)

Guidance literature:

With trifluoroacetic acid; In chloroform;

DOI:10.1039/P19720002873

Downstream raw materials:

D-glucose diethyl mercaptal

C₃₃H₃₈O₇S₃

1,2-di-O-acetyl-3,5,6-tri-O-benzoyl-β-D-glucofuranose

1,2-di-O-acetyl-3,5,6-tri-O-benzoyl-α-D-glucofuranose