Diethyl isocyanato succinate

Base Information

Chemical Name:Diethyl isocyanato succinate
CAS No.:17046-24-1
Molecular Formula:C₉H₁₃NO₅
Molecular Weight:215.206
Hs Code.:
NSC Number:514210
DSSTox Substance ID:DTXSID30325632
Mol file:17046-24-1.mol

Synonyms:17046-24-1;NSC 514210;Diethyl isocyanato succinate;DTXSID30325632;Diethyl N-(oxomethylidene)aspartate;NSC514210;NSC-514210

Suppliers and Price of Diethyl isocyanato succinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Diethyl isocyanato succinate

Chemical Property:

Vapor Pressure:0.00316mmHg at 25°C
Boiling Point:283.4°Cat760mmHg
Flash Point:118.2°C
Density:1.16g/cm³
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:215.07937252
Heavy Atom Count:15
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC(C(=O)OCC)N=C=O

Technology Process of Diethyl isocyanato succinate

There total 5 articles about Diethyl isocyanato succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 16115-68-7
diethyl L-aspartate hydrochloride

: 17046-24-1
N-carbonyl-L-aspartic acid diethyl ester

Guidance literature:: diethyl L-aspartate hydrochloride; With zinc; In dichloromethane; at 20 ℃;

phosgene; In dichloromethane; toluene; at 0 ℃;
DOI:10.1055/s-0030-1260216

Reference yield:

: 57471-70-2
diethyl N-benzyloxycarbonyl-(S)-aspartate

: 17046-24-1
N-carbonyl-L-aspartic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; hydrogen; acetic acid / water

2.1: zinc / dichloromethane / 20 °C

2.2: 0 °C

With hydrogenchloride; hydrogen; acetic acid; zinc; In dichloromethane; water;
DOI:10.1055/s-0030-1260216