3,4,5,6-tetrahydropyridin-2-ylcyanamide

Base Information

• Chemical Name: 3,4,5,6-tetrahydropyridin-2-ylcyanamide
• CAS No.: 97482-06-9
• Molecular Formula: C6H9N3
• Molecular Weight: 123.158

Synonyms:piperidin-2-ylidene-cyanamide;2-(N-Cyanimino)piperidine;N-(2-piperidinylidene)cyanamide;CYANAMIDE,(3,4,5,6-TETRAHYDRO-2-PYRIDINYL);(3,4,5,6-Tetrahydro-2-pyridinyl)cyanamide;

Chemical Property of 3,4,5,6-tetrahydropyridin-2-ylcyanamide

Chemical Property:

• Vapor Pressure: 0.245mmHg at 25°C
• Boiling Point: 205.8°C at 760 mmHg
• Flash Point: 78.3°C
• PSA: 48.18000
• Density: 1.15g/cm³
• LogP: 0.46598

Purity/Quality:

97% ^*data from raw suppliers

N-(2-PIPERIDINYLIDENE)CYANAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4,5,6-tetrahydropyridin-2-ylcyanamide

There total 3 articles about 3,4,5,6-tetrahydropyridin-2-ylcyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,3,4,5-tetrahydro-6-methoxypyridine (5693-62-9) + CYANAMID (420-04-2) → N-(piperidin-2-ylidene)cyanamide (97482-06-9)

Guidance literature:

In methanol; at 20 ℃; for 192h;

Reference yield: 91.0%

2,3,4,5-tetrahydro-6-methoxypyridine (5693-62-9) + CYANAMID (420-04-2) → 2-(N-Cyanimino)piperidine (97482-06-9)

Guidance literature:

In methanol; for 2h; Ambient temperature;

DOI:10.1007/BF00771771

Reference yield:

2,3,4,5-tetrahydro-6-methoxypyridine (5693-62-9) + CYANAMID (420-04-2) → piperidin-2-ylidene-cyanamide (97482-06-9)

Guidance literature:

In methanol; at 20 ℃; for 72.0833h;

upstream raw materials:

2,3,4,5-tetrahydro-6-methoxypyridine

CYANAMID

Downstream raw materials:

N-(1-(2-oxo-2-p-tolylethyl)piperidin-2-ylidene)cyanamide

2-(2-methyl-4-p-tolyl-5,6,7,8-tetrahydropyridino[1,2-b]imidazo[4,5-b]pyridin-3-yl)pentanoic acid

ethyl 2-(2-methyl-4-p-tolyl-5,6,7,8-tetrahydropyridino[1,2-b]imidazo[4,5-b]pyridin-3-yl)pentanoate

(2-amino-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-3-yl)(p-tolyl)methanone

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