(2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide

Base Information

• Chemical Name: (2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide
• CAS No.: 6662-53-9
• Molecular Formula: C8H6Cl2N2O2
• Molecular Weight: 233.054
• European Community (EC) Number: 652-158-0
• Mol file: 6662-53-9.mol

Synonyms:(2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide;1081809-48-4;N-(3,4-dichlorophenyl)-2-(N-hydroxyimino)acetamide;(2E)-N-(3,4-dichlorophenyl)-2-hydroxyiminoacetamide;(E)-N-(3,4-Dichlorophenyl)-2-(hydroxyimino)acetamide;(2E)-N-(3,4-DICHLOROPHENYL)-2-(N-HYDROXYIMINO)ACETAMIDE;starbld0012718;6662-53-9;SCHEMBL14341919;AKOS001042347;CS-0236875;EN300-17461;SR-01000390166;J-500779;SR-01000390166-1;Z56943361;(2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)ethanamide;(2E)-n-(3,4-dichlorophenyl)-2-(hydroxyimino)-acetamide

Chemical Property of (2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.49g/cm³
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 231.9806328
• Heavy Atom Count: 14
• Complexity: 235

Purity/Quality:

(2E)-N-(3,4-DICHLOROPHENYL)-2-(HYDROXYIMINO)ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1NC(=O)C=NO)Cl)Cl
• Isomeric SMILES: C1=CC(=C(C=C1NC(=O)/C=N/O)Cl)Cl

Technology Process of (2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide

There total 3 articles about (2E)-N-(3,4-dichlorophenyl)-2-(hydroxyimino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloral (75-87-6) + m,p-dichloroaniline (95-76-1) → N-(α-Oximino-acetyl)-3.4-dichlor-anilin (6662-53-9)

Guidance literature:

With hydroxylamine;

DOI:10.1021/jm00089a021

Reference yield:

chloral hydrate (302-17-0) + m,p-dichloroaniline (95-76-1) → N-(α-Oximino-acetyl)-3.4-dichlor-anilin (6662-53-9)

Guidance literature:

With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate; at 80 - 90 ℃; for 2h;

DOI:10.1021/jm031016d

Reference yield:

→ N-(α-Oximino-acetyl)-3.4-dichlor-anilin (6662-53-9)

Guidance literature:

aus entspr. Anilin (Sandmeyer-Rk.);

upstream raw materials:

chloral

m,p-dichloroaniline

chloral hydrate

Downstream raw materials:

4,5-Dichloro-1H-indole-2,3-dione

5,6-dichloroisatin

6-amino-2,3-dichlorobenzoic acid

2-amino-4,5-dichloro-benzoic acid

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