ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate

Base Information

Chemical Name:ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate
CAS No.:16992-94-2
Molecular Formula:C₁₈H₁₆O₄
Molecular Weight:296.323
Hs Code.:
NSC Number:159433
DSSTox Substance ID:DTXSID20303626
Mol file:16992-94-2.mol

Synonyms:16992-94-2;NSC159433;ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate;DTXSID20303626;NSC-159433

Suppliers and Price of ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate

Chemical Property:

Vapor Pressure:1.28E-09mmHg at 25°C
Boiling Point:486.6°C at 760 mmHg
Flash Point:216.8°C
Density:1.262g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:296.10485899
Heavy Atom Count:22
Complexity:470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=O)C1CCC2=C(C1=O)C=CC3=CC=CC=C23

Technology Process of ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate

There total 2 articles about ethyl 2-oxo-2-(1-oxo-3,4-dihydro-2H-phenanthren-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 573-22-8
3,4-dihydro-2H-phenanthren-1-one

: 95-92-1
oxalic acid diethyl ester

: 16992-94-2
Ethyl 1-oxo-1,2,3,4-tetrahydrophenanthrene-2-glyoxalate

Guidance literature:: With sodium ethanolate; In benzene; for 7h; Ambient temperature;

Reference yield:

: 781-74-8
4-(1-naphthyl)butanoic acid

: 16992-94-2
Ethyl 1-oxo-1,2,3,4-tetrahydrophenanthrene-2-glyoxalate

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / PPA

2: 62 percent / NaOEt / benzene / 7 h / Ambient temperature

With sodium ethanolate; In benzene;