Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane

Base Information

Chemical Name:Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane
CAS No.:917-20-4
Molecular Formula:C46H50 P2 . 2 Br
Molecular Weight:824.64
Hs Code.:
European Community (EC) Number:651-755-3
UNII:YJJ33U9L0U
Mol file:917-20-4.mol

Synonyms:917-20-4;Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane;1,10-DECAMETHYLENEBIS(TRIPHENYLPHOSPHONIUM BROMIDE);NSC 84075;YJJ33U9L0U;DECAPHOSPHENONIUM BROMIDE;triphenyl(10-triphenylphosphaniumyldecyl)phosphanium;dibromide;Decane-1,10-diylbis(triphenylphosphonium) bromide;NSC-84075;UNII-YJJ33U9L0U;AKOS024427453;PHOSPHONIUM, 1,1'-(1,10-DECANEDIYL)BIS(1,1,1-TRIPHENYL-, BROMIDE (1:2)

Suppliers and Price of Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,10-DECAMETHYLENEBIS(TRIPHENYLPHOSPHONIUM BROMIDE) 95.00%
5MG
$ 505.30

Total 7 raw suppliers

Chemical Property of Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：27.18000
Density:g/cm³
LogP:4.10340
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:17
Exact Mass:824.17340
Heavy Atom Count:50
Complexity:669

Purity/Quality:

99% ^*data from raw suppliers

1,10-DECAMETHYLENEBIS(TRIPHENYLPHOSPHONIUM BROMIDE) 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[P+](CCCCCCCCCC[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6.[Br-].[Br-]

Technology Process of Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane

There total 2 articles about Triphenyl(10-(triphenylphosphoranyl)decyl)phosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4101-68-2
1,10-dibromodecane

: 603-35-0
triphenylphosphine

: 917-20-4
Decamethylene-1,10-bis(triphenylphosphonium bromide)

Guidance literature:: In acetonitrile; at 100 ℃; for 30h;
DOI:10.1016/0009-3084(96)02537-6

Reference yield:

: 917-20-4
Decamethylene-1,10-bis(triphenylphosphonium bromide)

Guidance literature:: /BRN= 3875042/;

Reference yield: 30.0%

: 10458-14-7,14073-97-3,17627-49-5,7786-64-3
(2R,5S)-menthone

: 917-20-4
Decamethylene-1,10-bis(triphenylphosphonium bromide)

: (1E,10E)-1,10-bis[(2S,5R)-2-isopropyl-5-methylcyclohexylidene]decane

Guidance literature:: Decamethylene-1,10-bis(triphenylphosphonium bromide); With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

(2R,5S)-menthone; In tetrahydrofuran; at 20 ℃; for 72h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201900177