3-[4-[2-hydroxy-3-(tert-butylamino)propoxy]phenyl]-1-methyl-urea

Base Information

• Chemical Name: 3-[4-[2-hydroxy-3-(tert-butylamino)propoxy]phenyl]-1-methyl-urea
• CAS No.: 38649-71-7
• Molecular Formula: C₁₅H₂₅N₃O₃
• Molecular Weight: 295.382
• Mol file: 38649-71-7.mol

Synonyms:1-[4-(3-Methylureido)phenoxy]-3-(tert-butylamino)-2-propanol

Chemical Property of 3-[4-[2-hydroxy-3-(tert-butylamino)propoxy]phenyl]-1-methyl-urea

Chemical Property:

• Vapor Pressure: 8.4E-09mmHg at 25°C
• Boiling Point: 447.8°Cat760mmHg
• Flash Point: 224.6°C
• PSA: 86.11000
• Density: 1.131g/cm³
• LogP: 2.23400

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-[4-[2-hydroxy-3-(tert-butylamino)propoxy]phenyl]-1-methyl-urea

There total 3 articles about 3-[4-[2-hydroxy-3-(tert-butylamino)propoxy]phenyl]-1-methyl-urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-aminophenol hydrochloride (51-78-5) → 1-[4-(3-tert-Butylamino-2-hydroxy-propoxy)-phenyl]-3-methyl-urea (38649-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂CO₃

2: aq. NaOH

With sodium hydroxide; sodium carbonate;

Reference yield:

2-methyl-N-(oxiran-2-ylmethyl)propan-2-amine (13080-65-4) + 1-(4-hydroxyphenyl)-3-methylurea (38652-14-1) → 1-[4-(3-tert-Butylamino-2-hydroxy-propoxy)-phenyl]-3-methyl-urea (38649-71-7)

Guidance literature:

With sodium hydroxide;

Reference yield:

→ 1-[4-(3-tert-Butylamino-2-hydroxy-propoxy)-phenyl]-3-methyl-urea (38649-71-7)

Guidance literature:

4-(3-Methylureido)-phenol 1. Epichlorhydrin 2. t-Butylamin;

DOI:10.1021/jm00215a017

upstream raw materials:

2-methyl-N-(oxiran-2-ylmethyl)propan-2-amine

1-(4-hydroxyphenyl)-3-methylurea

p-aminophenol hydrochloride

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