Technology Process of Naphthalene, undecyl-
There total 7 articles about Naphthalene, undecyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine N-oxide; potassium fluoride; 1,10-Phenanthroline; lithium chloride; nickel dichloride; zinc;
In
N,N-dimethyl acetamide;
at 0 ℃;
for 72h;
Inert atmosphere;
DOI:10.1016/j.tet.2019.05.070
- Guidance literature:
-
With
copper oxide-chromium oxide;
at 250 - 280 ℃;
under 84583.4 Torr;
Hydrogenation.Erhitzen des Reaktionsprodukts mit Palladium/Kohle auf 280grad;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 20 °C
2.1: triethylamine / dichloromethane / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: nickel dichloride; pyridine N-oxide; 1,10-Phenanthroline; potassium fluoride; zinc; lithium chloride / N,N-dimethyl acetamide / 72 h / 0 °C / Inert atmosphere
With
pyridine N-oxide; potassium fluoride; 1,10-Phenanthroline; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; lithium chloride; nickel dichloride; zinc;
In
dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.tet.2019.05.070
