1-(p-Toluenesulfonyl)azetidine

Base Information

Chemical Name:1-(p-Toluenesulfonyl)azetidine
CAS No.:7730-45-2
Molecular Formula:C10H13NO2S
Molecular Weight:211.285
Hs Code.:2933990090
NSC Number:143590
DSSTox Substance ID:DTXSID80301461
Nikkaji Number:J105.138E
Wikidata:Q82045411
Mol file:7730-45-2.mol

Synonyms:1-(p-Toluenesulfonyl)azetidine;7730-45-2;1-Tosylazetidine;N-p-Tosylazetidine;1-(p-Tolylsulfonyl)azetidine;1-(4-methylphenyl)sulfonylazetidine;1-[(4-Methylphenyl)sulfonyl]azetidine;Azetidine, 1-(p-tolylsulfonyl)-;Azetidine, 1-[(4-methylphenyl)sulfonyl]-;N-tosyl azetidine;1-(4-methylbenzenesulfonyl)azetidine;NSC143590;CBDivE_013213;M-TOLUIDINEHYDROCHLORIDE;SCHEMBL10409988;DTXSID80301461;VKCBXONEZGIOSP-UHFFFAOYSA-N;STK324706;1-(p-Toluenesulfonyl)azetidine, 97%;AKOS000591525;NSC-143590;FT-0636582;AB00073626-01;SR-01000317261;SR-01000317261-1

Suppliers and Price of 1-(p-Toluenesulfonyl)azetidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
1-(p-Toluenesulfonyl)azetidine 97%
1g
$ 114.00

American Custom Chemicals Corporation
1-(P-TOLUENESULFONYL)AZETIDINE 95.00%
1G
$ 660.59

AK Scientific
1-(p-Toluenesulfonyl)azetidine
1g
$ 135.00

Total 11 raw suppliers

Chemical Property of 1-(p-Toluenesulfonyl)azetidine

Chemical Property:

Vapor Pressure:0.000104mmHg at 25°C
Melting Point:119-122oC(lit.)
Boiling Point:337.6°Cat760mmHg
Flash Point:158°C
PSA：45.76000
Density:1.276g/cm³
LogP:2.40810
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:211.06669983
Heavy Atom Count:14
Complexity:282

Purity/Quality:

98%min ^*data from raw suppliers

1-(p-Toluenesulfonyl)azetidine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2CCC2

Technology Process of 1-(p-Toluenesulfonyl)azetidine

There total 19 articles about 1-(p-Toluenesulfonyl)azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 143590-74-3
4-Methyl-N-(3-phenylselanyl-propyl)-benzenesulfonamide

: 7730-45-2
1-(toluene-4-sulfonyl)azetidine

Guidance literature:: With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In ethanol; for 1h; Ambient temperature;
DOI:10.1016/0040-4039(92)88089-N

Reference yield: 92.0%

: 98-59-9
p-toluenesulfonyl chloride

: azetidine hydrogen perchlorate

: 7730-45-2
1-(toluene-4-sulfonyl)azetidine

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; 1.) 0 deg C, 30 min, 2.) RT, 1 h;
DOI:10.1002/jhet.5570300506

Reference yield: 85.0%

: 653-37-2
perfluorobenzaldehyde

: 3245-95-2
N-(3-bromo-propyl)-4-methyl-benzenesulfonamide

: 7730-45-2
1-(toluene-4-sulfonyl)azetidine

: 10019-95-1
N-tosylpyrrolidinone

Guidance literature:: With potassium carbonate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; 1,3-bis-(diphenylphosphino)propane; In xylene; at 130 ℃; for 18h;
DOI:10.1016/j.jorganchem.2006.08.038