3-Benzoylquinoline

Base Information

• Chemical Name: 3-Benzoylquinoline
• CAS No.: 37045-14-0
• Molecular Formula: C16H11NO
• Molecular Weight: 233.269
• Hs Code.: 2933499090
• Mol file: 37045-14-0.mol

Synonyms:3-Benzoylquinoline;[3]Chinolyl-phenyl-keton;phenyl-3-quinolinyl-methanone;phenylquinolin-3-ylmethanone;[3]quinolyl-phenyl ketone;

Chemical Property of 3-Benzoylquinoline

Chemical Property:

• Vapor Pressure: 1.2E-06mmHg at 25°C
• Boiling Point: 401.3°Cat760mmHg
• Flash Point: 203.1°C
• PSA: 29.96000
• Density: 1.196g/cm³
• LogP: 3.46580

Purity/Quality:

98%+ ^*data from raw suppliers

3-Benzoylquinoline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Benzoylquinoline

There total 37 articles about 3-Benzoylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-Iodoquinoline (79476-07-6) + carbon monoxide (201230-82-2) + phenylboronic acid (98-80-6) → phenyl(quinolin-3-yl)methanone (37045-14-0)

Guidance literature:

3-Iodoquinoline; phenylboronic acid; With potassium carbonate; In toluene; for 0.166667h; Autoclave;

carbon monoxide; In toluene; at 100 ℃; for 10h; under 10343.2 Torr; Autoclave;

DOI:10.1055/s-0030-1258349

Reference yield: 95.0%

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide (6590-65-4) + phenyl propargyl ketone (3623-15-2) → phenyl(quinolin-3-yl)methanone (37045-14-0)

Guidance literature:

N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide; phenyl propargyl ketone; With triphenylphosphine; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

With hydrogenchloride; In water; acetonitrile; for 0.0833333h; Inert atmosphere;

DOI:10.1021/jo3015825

Reference yield: 95.0%

3-quinolylcarboxaldehyde (13669-42-6) + phenylboronic acid (98-80-6) → phenyl(quinolin-3-yl)methanone (37045-14-0)

Guidance literature:

3-quinolylcarboxaldehyde; phenylboronic acid; With 1-(2,6-diisopropylphenyl)-3-(2-(phenylthio)phenyl)-4,5-dihydroimidazolinium chloride; bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; In 1,4-dioxane; at 100 ℃; for 1h; Inert atmosphere;

With ortho-methylphenyl iodide; In 1,4-dioxane; at 100 ℃; for 15h; Inert atmosphere;

DOI:10.1002/ejoc.201300269

upstream raw materials:

quinoline-3-carbonyl chloride

benzene

3-bromoquinoline

phenylacetonitrile

Downstream raw materials:

phenyl(4-phenylquinolin-3-yl)methanone

3-phenylquinoline

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