Technology Process of Oxotriphenoxyvanadium
There total 2 articles about Oxotriphenoxyvanadium which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
benzene;
byproducts: HCl; mixing VOCl3 and phenol, refluxing in benzene for a few hours; sepn. of product, filtn. of contact with air, washing with benzene followed by hexane, drying in vacuo at 40°C, elem. anal.;
- Guidance literature:
-
In
neat (no solvent);
heating;; pptn.;;