1,1',1''-Methanetriyltris(2-methylbenzene)

Base Information

Chemical Name:1,1',1''-Methanetriyltris(2-methylbenzene)
CAS No.:6270-89-9
Molecular Formula:C22H22
Molecular Weight:286.417
Hs Code.:
NSC Number:36367
DSSTox Substance ID:DTXSID40284261
Wikidata:Q82019140

Synonyms:6270-89-9;1,1',1''-methanetriyltris(2-methylbenzene);Tritoluylmethan;NSC36367;DTXSID40284261;NSC-36367

Suppliers and Price of 1,1',1''-Methanetriyltris(2-methylbenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 1,1',1''-Methanetriyltris(2-methylbenzene)

Chemical Property:

Boiling Point:405.9 °C at 760 mmHg
Flash Point:195.8 °C
Density:1.017 g/cm³
XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:286.172150702
Heavy Atom Count:22
Complexity:281

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(C2=CC=CC=C2C)C3=CC=CC=C3C

Technology Process of 1,1',1''-Methanetriyltris(2-methylbenzene)

There total 5 articles about 1,1',1''-Methanetriyltris(2-methylbenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6922-86-7
tris(o-methylphenyl)methanol

: 6270-89-9
tri-o-tolylphosphine

Guidance literature:: With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; for 2.5h; Cooling with ice;

Reference yield:

: 717102-41-5
2-(2,2'-dimethyl-benzhydryl)-benzaldehyde

: 6270-89-9
tri-o-tolylphosphine

Guidance literature:: With ethanol; sodium ethanolate; hydrazine hydrate; at 200 - 210 ℃;
DOI:10.1021/ja01260a027

Reference yield:

: 75195-51-6
3,3-O-di-o-tolyl-1,3-dihydro-2-benzofuran-1-one

: 6270-89-9
tri-o-tolylphosphine

Guidance literature:: Multi-step reaction with 4 steps

1: copper oxide-chromium oxide / 235 - 250 °C / 119888 Torr / Hydrogenation

2: ueber das Saeurechlorid

3: PCl₅; toluene / Behandeln des Reaktionsprodukts mit SnCl₂ und HCl in Aether bei 0grad und Erhitzen der erhaltenen orangeroten Krystalle mit wss. HCl

4: aqueous hydrazine; sodium ethylate; ethanol / 200 - 210 °C

With ethanol; copper oxide-chromium oxide; phosphorus pentachloride; sodium ethanolate; hydrazine hydrate; toluene;
DOI:10.1021/ja01260a027