Technology Process of 2-hydroxy-4-[(2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy]-3,6-dimethylbenzoic acid
There total 11 articles about 2-hydroxy-4-[(2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy]-3,6-dimethylbenzoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 55 percent / NaOCH2Ph / 24 h / Heating
2: 69 percent / (CF3-CO)2O / toluene / 20 °C
3: H2; 10 percent Pd/C / ethyl acetate
With
palladium on activated charcoal; hydrogen; sodium phenyl-methanolate; trifluoroacetic anhydride;
In
ethyl acetate; toluene;
1: transesterification / 2: Esterification / 3: Hydrogenolysis;
DOI:10.1016/S0223-5234(99)00132-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 69 percent / (CF3-CO)2O / toluene / 20 °C
2: H2; 10 percent Pd/C / ethyl acetate
With
palladium on activated charcoal; hydrogen; trifluoroacetic anhydride;
In
ethyl acetate; toluene;
1: Esterification / 2: Hydrogenolysis;
DOI:10.1016/S0223-5234(99)00132-4
