benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate

Base Information

• Chemical Name: benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate
• CAS No.: 56410-44-7
• Molecular Formula: C₂₆H₂₆O₇
• Molecular Weight: 450.488
• Mol file: 56410-44-7.mol

Synonyms:benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate

Chemical Property of benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate

There total 9 articles about benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-hydroxy-4-methoxy-3,6-dimethylbenzoic acid (479-26-5) + benzyl 2,4-dihydroxy-3,6-dimethylbenzoate (56410-30-1) → benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate (56410-44-7)

Guidance literature:

With trifluoroacetic anhydride; In toluene; at 20 ℃;

DOI:10.1016/S0223-5234(99)00132-4

Reference yield:

ethyl 2,4-dihydroxy-3,6-dimethylbenzoate (31581-32-5) → benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate (56410-44-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / NaOCH₂Ph / 24 h / Heating

2: 69 percent / (CF₃-CO)2O / toluene / 20 °C

With sodium phenyl-methanolate; trifluoroacetic anhydride; In toluene; 1: transesterification / 2: Esterification;

DOI:10.1016/S0223-5234(99)00132-4

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) → benzyl 2-hydroxy-4-((2-hydroxy-4-methoxy-3,6-dimethylbenzoyl)oxy)-3,6-dimethyl benzoate (56410-44-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / NaOCH₂Ph / 24 h / Heating

2: 69 percent / (CF₃-CO)2O / toluene / 20 °C

With sodium phenyl-methanolate; trifluoroacetic anhydride; In toluene; 1: transesterification / 2: Esterification;

DOI:10.1016/S0223-5234(99)00132-4

upstream raw materials:

2-hydroxy-4-methoxy-3,6-dimethylbenzoic acid

benzyl 2,4-dihydroxy-3,6-dimethylbenzoate

ethyl 2,4-dihydroxy-3,6-dimethylbenzoate

benzyl alcohol

Downstream raw materials:

barbatic acid