tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate

Base Information

• Chemical Name: tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate
• CAS No.: 93042-56-9
• Molecular Formula: C₁₂H₁₅N₃O₅
• Molecular Weight: 281.268
• DSSTox Substance ID: DTXSID30409244
• NSC Number: 109951
• Wikidata: Q82214986
• Mol file: 93042-56-9.mol

Synonyms:93042-56-9;NSC109951;tert-butyl N-[(4-nitrobenzoyl)amino]carbamate;SCHEMBL6816134;tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate;DTXSID30409244;AKOS003245665;NSC-109951;SR-01000220041;tert-butyl 2-(4-nitrobenzoyl)hydrazinecarboxylate;SR-01000220041-1;Z32379826

Chemical Property of tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.278g/cm³
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 281.10117059
• Heavy Atom Count: 20
• Complexity: 378

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)OC(=O)NNC(=O)C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate

There total 2 articles about tert-Butyl 2-(4-nitrobenzoyl)hydrazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butoxycarbonylhydrazine (870-46-2) + 4-nitro-benzoyl chloride (122-04-3) → tert.-Butyl-2-<4-nitro-benzoyl>-carbazet (93042-56-9)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 5h;

DOI:10.3390/molecules24244440

Reference yield:

N-(tert-butyloxycarbonyl) azide (1070-19-5) + 4-nitro-benzoyl chloride (122-04-3) → tert.-Butyl-2-<4-nitro-benzoyl>-carbazet (93042-56-9)

Guidance literature:

With pyridine; In dichloromethane;

DOI:10.1021/jo01069a037

Reference yield:

tert.-Butyl-2-<4-nitro-benzoyl>-carbazet (93042-56-9) → 4-nitrobenzoyliminoamine monohydrochloride

Guidance literature:

With hydrogenchloride; In methanol; at 0 ℃; for 1h;

DOI:10.3390/molecules24244440

upstream raw materials:

N-(tert-butyloxycarbonyl) azide

4-nitro-benzoyl chloride

t-butoxycarbonylhydrazine