1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine

Base Information

Chemical Name:1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine
CAS No.:89159-81-9
Molecular Formula:C27H29N
Molecular Weight:367.5259
Hs Code.:
DSSTox Substance ID:DTXSID001008675

Synonyms:BRN 5762461;1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine;1-(3'-Phenylpropyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine;Pyridine, 1,2,5,6-tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)-;89159-81-9;C27H29N;DTXSID001008675;C27-H29-N;LS-132015;5-Methyl-4,6-diphenyl-1-(3-phenylpropyl)-1,2,3,6-tetrahydropyridine

Suppliers and Price of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine

Chemical Property:

Vapor Pressure:8.4E-11mmHg at 25°C
Boiling Point:517.2°Cat760mmHg
Flash Point:230.6°C
Density:1.05g/cm³
XLogP3:6.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:367.229999929
Heavy Atom Count:28
Complexity:488

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CCN(C1C2=CC=CC=C2)CCCC3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine

There total 5 articles about 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 89159-79-5
1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

: 89159-81-9
1-(3'-Phenylpropyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: With hydrogen; nickel; In ethanol; for 2.33333h;
DOI:10.1007/BF00764173

Reference yield:

: 591-51-5
phenyllithium

: 89159-81-9
1-(3'-Phenylpropyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

3: 84 percent / H₂ / 5percent Pd/CaCO₃ / ethanol

4: 97 percent / H₂, Raney nickel / ethanol / 2.33 h

With PPA; hydrogen; nickel; propionic acid; propionic acid anhydride; Lindlar's catalyst; In diethyl ether; ethanol;
DOI:10.1007/BF00764173

Reference yield:

: 63445-66-9,89159-74-0
(2R,3S)-3-Methyl-2-phenyl-1-(3-phenyl-prop-2-ynyl)-piperidin-4-one

: 89159-81-9
1-(3'-Phenylpropyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

3: 84 percent / H₂ / 5percent Pd/CaCO₃ / ethanol

4: 97 percent / H₂, Raney nickel / ethanol / 2.33 h

With PPA; hydrogen; nickel; propionic acid; propionic acid anhydride; Lindlar's catalyst; In diethyl ether; ethanol;
DOI:10.1007/BF00764173