1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine

Base Information

Chemical Name:1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine
CAS No.:89159-77-3
Molecular Formula:C30H31N
Molecular Weight:405.5738
Hs Code.:
DSSTox Substance ID:DTXSID301008674

Synonyms:BRN 5763587;1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine;1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine;Pyridine, 1,2,5,6-tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)-;89159-77-3;C27H25N;DTXSID301008674;LS-132016;5-Methyl-4,6-diphenyl-1-(6-phenylhex-1-yn-3-yl)-1,2,3,6-tetrahydropyridine

Suppliers and Price of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine

Chemical Property:

Vapor Pressure:2.49E-12mmHg at 25°C
Boiling Point:554.4°Cat760mmHg
Flash Point:247.4°C
Density:1.063g/cm³
XLogP3:6.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:405.245649993
Heavy Atom Count:31
Complexity:618

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CCN(C1C2=CC=CC=C2)C(CCCC3=CC=CC=C3)C#C)C4=CC=CC=C4

Technology Process of 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine

There total 3 articles about 1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenylpropyl-2-propynyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 89159-75-1
1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-4-hydroxypiperidine

: 89159-77-3
1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: With PPA; propionic acid; propionic acid anhydride; for 12h; Ambient temperature;
DOI:10.1007/BF00764173

Reference yield:

: 591-51-5
phenyllithium

: 89159-77-3
1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

With PPA; propionic acid; propionic acid anhydride; In diethyl ether;
DOI:10.1007/BF00764173

Reference yield:

: 63445-66-9,89159-74-0
(2R,3S)-3-Methyl-2-phenyl-1-(3-phenyl-prop-2-ynyl)-piperidin-4-one

: 89159-77-3
1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

With PPA; propionic acid; propionic acid anhydride; In diethyl ether;
DOI:10.1007/BF00764173