1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Base Information

Chemical Name:1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine
CAS No.:89159-79-5
Molecular Formula:C27H27N
Molecular Weight:365.51
Hs Code.:

Synonyms:BRN 5760180;1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine;1,2,5,6-Tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenyl-2-propenyl)pyridine;Pyridine, 1,2,5,6-tetrahydro-2,4-diphenyl-3-methyl-1-(3-phenyl-2-propenyl)-;89159-79-5;C27H27N;C27-H27-N;LS-132014

Suppliers and Price of 1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Chemical Property:

Vapor Pressure:3.03E-11mmHg at 25°C
Boiling Point:528.2°Cat760mmHg
Flash Point:235.6°C
Density:1.07g/cm³
XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:365.214349865
Heavy Atom Count:28
Complexity:527

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CCN(C1C2=CC=CC=C2)CC=CC3=CC=CC=C3)C4=CC=CC=C4
Isomeric SMILES:CC1=C(CCN(C1C2=CC=CC=C2)C/C=C/C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

There total 4 articles about 1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 89159-77-3
1-(3'-Phenyl-2'-propynyl)-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

: 89159-79-5
1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol;
DOI:10.1007/BF00764173

Reference yield:

: 591-51-5
phenyllithium

: 89159-79-5
1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

3: 84 percent / H₂ / 5percent Pd/CaCO₃ / ethanol

With PPA; hydrogen; propionic acid; propionic acid anhydride; Lindlar's catalyst; In diethyl ether; ethanol;
DOI:10.1007/BF00764173

Reference yield:

: 63445-66-9,89159-74-0
(2R,3S)-3-Methyl-2-phenyl-1-(3-phenyl-prop-2-ynyl)-piperidin-4-one

: 89159-79-5
1-Cinnamyl-2,4-diphenyl-3-methyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / diethyl ether / 24 h / Ambient temperature

2: 95 percent / propionic anhydride, propionic acid, polyphosphoric acid / 12 h / Ambient temperature

3: 84 percent / H₂ / 5percent Pd/CaCO₃ / ethanol

With PPA; hydrogen; propionic acid; propionic acid anhydride; Lindlar's catalyst; In diethyl ether; ethanol;
DOI:10.1007/BF00764173