(2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine

Base Information

Chemical Name:(2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine
CAS No.:63452-43-7
Molecular Formula:C16H18N2O3
Molecular Weight:286.331
Hs Code.:
NSC Number:230414

Synonyms:NSC230414;NSC-230414;SR-01000106518;SR-01000106518-1;(2E)-1-PHENYL-2-[(3,4,5-TRIMETHOXYPHENYL)METHYLIDENE]HYDRAZINE

Suppliers and Price of (2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine

Chemical Property:

Vapor Pressure:1.92E-07mmHg at 25°C
Boiling Point:425.4°Cat760mmHg
Flash Point:211.1°C
Density:1.1g/cm³
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:286.13174244
Heavy Atom Count:21
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC)OC)C=NNC2=CC=CC=C2
Isomeric SMILES:COC1=CC(=CC(=C1OC)OC)/C=N/NC2=CC=CC=C2

Technology Process of (2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine

There total 3 articles about (2E)-1-Phenyl-2-[(3,4,5-trimethoxyphenyl)methylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 100-63-0
phenylhydrazine

: 63452-43-7
1-phenyl-2-(3,4,5-trimethoxybenzylidene)hydrazine

Guidance literature:: magnesium(II) perchlorate; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1016/j.tetlet.2004.08.097

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 63452-43-7
1-phenyl-2-(3,4,5-trimethoxybenzylidene)hydrazine

Guidance literature:: With sodium acetate; In ethanol; water; at 20 - 80 ℃;
DOI:10.1021/jo2005632

Reference yield:

: 62-53-3
aniline

: 63452-43-7
1-phenyl-2-(3,4,5-trimethoxybenzylidene)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: sodium acetate / ethanol; water / 20 - 80 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In ethanol; water;
DOI:10.1021/jo2005632