3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-

Base Information

Chemical Name:3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-
CAS No.:130403-15-5
Molecular Formula:C₁₄H₁₆N₂O₃
Molecular Weight:260.293
Hs Code.:
DSSTox Substance ID:DTXSID70156523
Nikkaji Number:J517.260H
Wikidata:Q83024594

Synonyms:BRN 5822047;130403-15-5;3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-;N-(4-Methoxy-2,6-dimethylphenyl)-5-methyl-3-isoxazolecarboxamide;DTXSID70156523;LS-86564;5-Methyl-N-(2,6-dimethyl-4-methoxyphenyl)isoxazole-3-carboxamide

Suppliers and Price of 3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-

Chemical Property:

Vapor Pressure:4.23E-05mmHg at 25°C
Boiling Point:351°Cat760mmHg
Flash Point:166.1°C
Density:1.198g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:260.11609238
Heavy Atom Count:19
Complexity:312

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1NC(=O)C2=NOC(=C2)C)C)OC

Technology Process of 3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl-

There total 2 articles about 3-Isoxazolecarboxamide, N-(4-methoxy-2,6-dimethylphenyl)-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37621-81-1
sodium 3,5-dimethylphenolate

: 130403-15-5
5-Methyl-isoxazole-3-carboxylic acid (4-methoxy-2,6-dimethyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na₂CO₃, sulfanilic acid, NaNO₂, 2.) 85percent aq. sodium hydrosulfite / 1.) water, a.) RT, overnight, b.) 40 deg C, 3 h, 2.) water, 60 deg C, 1 h

2: Et₃N / toluene / 4 h / Heating

With sodium disulfite; sodium carbonate; triethylamine; sodium nitrite; 4-aminobenzene sulfonic acid; In toluene;
DOI:10.1016/0223-5234(92)90137-P