2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate

Base Information

Chemical Name:2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate
CAS No.:117036-93-8
Molecular Formula:C13H16O5S
Molecular Weight:284.333
Hs Code.:
DSSTox Substance ID:DTXSID10553673
Wikidata:Q82434320
Mol file:117036-93-8.mol

Synonyms:117036-93-8;2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate;DTXSID10553673

Suppliers and Price of 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:284.07184478
Heavy Atom Count:19
Complexity:401

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)OCC(=C)CS(=O)(=O)C1=CC=CC=C1

Technology Process of 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate

There total 4 articles about 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 541-41-3
chloroformic acid ethyl ester

: 117037-30-6
3-hydroxy 2-methylene propanesulfonyl benzene

: 117036-93-8
ethyl 2-(benzenesulfonylmethyl)-2-propenyl carbonate

Guidance literature:: With pyridine; In diethyl ether; at 0 - 10 ℃; for 24h;

Reference yield:

: 49639-05-6
1-(phenylsulfonyl)-2-methyl-2-propene

: 117036-93-8
ethyl 2-(benzenesulfonylmethyl)-2-propenyl carbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / sulfuryl cloride / CH₂Cl₂ / Heating; 1.) 15 min; 2.) reflux 30 min

2: 100 percent / formic acid / 48 h / Heating

3: 63 percent / 1N HCl / methanol / Ambient temperature

4: 87 percent / pyridine / diethyl ether / 24 h / 0 - 10 °C

With pyridine; hydrogenchloride; formic acid; sulfuryl dichloride; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 116830-92-3
2-(chloromethyl)-3-(phenylsulfonyl)-1-propene

: 117036-93-8
ethyl 2-(benzenesulfonylmethyl)-2-propenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / formic acid / 48 h / Heating

2: 63 percent / 1N HCl / methanol / Ambient temperature

3: 87 percent / pyridine / diethyl ether / 24 h / 0 - 10 °C

With pyridine; hydrogenchloride; formic acid; In methanol; diethyl ether;