Technology Process of 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate
There total 4 articles about 2-[(Benzenesulfonyl)methyl]prop-2-en-1-yl ethyl carbonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
diethyl ether;
at 0 - 10 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 58 percent / sulfuryl cloride / CH2Cl2 / Heating; 1.) 15 min; 2.) reflux 30 min
2: 100 percent / formic acid / 48 h / Heating
3: 63 percent / 1N HCl / methanol / Ambient temperature
4: 87 percent / pyridine / diethyl ether / 24 h / 0 - 10 °C
With
pyridine; hydrogenchloride; formic acid; sulfuryl dichloride;
In
methanol; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / formic acid / 48 h / Heating
2: 63 percent / 1N HCl / methanol / Ambient temperature
3: 87 percent / pyridine / diethyl ether / 24 h / 0 - 10 °C
With
pyridine; hydrogenchloride; formic acid;
In
methanol; diethyl ether;