tris[2-(dimethylamino)ethyl] borate

Base Information

• Chemical Name: tris[2-(dimethylamino)ethyl] borate
• CAS No.: 97-21-2
• Molecular Formula: C₁₂H₃₀BN₃O₃
• Molecular Weight: 275.2
• Mol file: 97-21-2.mol

Synonyms:Boric acid(H3BO3), tris[2-(dimethylamino)ethyl] ester (9CI); Ethanol, 2-(dimethylamino)-,borate (7CI); Ethanol, 2-(dimethylamino)-, triester with boric acid (H3BO3)(8CI); NSC 146257; Tris(2-dimethylaminoethoxy)borane

Chemical Property of tris[2-(dimethylamino)ethyl] borate

Chemical Property:

• Vapor Pressure: 0.00214mmHg at 25°C
• Boiling Point: 289.9°Cat760mmHg
• Flash Point: 129.1°C
• Density: 0.95g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tris[2-(dimethylamino)ethyl] borate

There total 3 articles about tris[2-(dimethylamino)ethyl] borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(N,N-dimethylamino)ethanol (108-01-0) → tris[2-(dimethylamino)ethyl] borate (97-21-2)

Guidance literature:

With Trimethyl borate; at 50 ℃;

DOI:10.1007/s11172-008-0259-5

Reference yield: 99.0%

2-(N,N-dimethylamino)ethanol (108-01-0) + Trimethyl borate (121-43-7,63156-11-6) → tris[2-(dimethylamino)ethyl] borate (97-21-2)

Guidance literature:

In neat (no solvent); mixt. was stirred at 50°C; volatiles were removed under reduced pressure; NMR;

DOI:10.1007/s11172-008-0259-5

Reference yield:

→ tris[2-(dimethylamino)ethyl] borate (97-21-2)

Guidance literature:

Methylborat, 2-(N,N-Dimethylamino)ethanol;

DOI:10.1021/ic50037a025

upstream raw materials:

2-(N,N-dimethylamino)ethanol

Trimethyl borate

Downstream raw materials:

N,N-dimethyl-2-[(6-methyl-4,4-diphenyl-1,3,6,2-dioxazaborocan-2-yl)oxy]ethaneamine