d-Bulbocapnine

Base Information

• Chemical Name: d-Bulbocapnine
• CAS No.: 72002-80-3
• Molecular Formula: C19H19NO4
• Molecular Weight: 325.364
• DSSTox Substance ID: DTXSID50871626
• Wikidata: Q105154650
• Metabolomics Workbench ID: 67622

Synonyms:d-Bulbocapnine;5H-Benzo(g)-1,3-benzodioxolo(6,5,4-de)quinolin-12-ol, 6,7,7a,8-tetrahydro-11-methoxy-7-methyl-;(S)-(+)-Bulbocapnine;72002-80-3;Bulbokapnin;Oprea1_003816;SCHEMBL11253583;ACon1_002350;DTXSID50871626;LODGIKWNLDQZBM-UHFFFAOYSA-N;NCGC00169929-01;LS-21496;BRD-A35379089-001-01-6;6a.alpha.-Aporphin-11-ol, 10-methoxy-1,2-(methylenedioxy)-;11-Methoxy-7-methyl-6,7,7a,8-tetrahydro-2H,5H-[1,3]benzodioxolo[6,5,4-de]benzo[g]quinolin-12-ol;11-Methoxy-7-methyl-6,7,7a,8-tetrahydro-5H-[1,3]benzodioxolo[6,5,4-de]benzo[g]quinolin-12-ol, (S)-

Chemical Property of d-Bulbocapnine

Chemical Property:

• Boiling Point: 504°Cat760mmHg
• Flash Point: 258.6°C
• Density: 1.342g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 1
• Exact Mass: 325.13140809
• Heavy Atom Count: 24
• Complexity: 488

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1CCC2=CC3=C(C4=C2C1CC5=C4C(=C(C=C5)OC)O)OCO3

Technology Process of d-Bulbocapnine

There total 3 articles about d-Bulbocapnine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+-)-bulbocapnine (72002-80-3) → (S)-bulocapnine (298-45-3,7773-42-4,71959-13-2,72002-80-3)

Guidance literature:

With D-tartaric acid;

Reference yield:

→ (S)-bulocapnine (298-45-3,7773-42-4,71959-13-2,72002-80-3)

Guidance literature:

Reference yield:

→ (+/-)-1-(3-hydroxy-4-methoxybenzyl)-1,2,3,4-tetrahydro-2-methyl-6,7-methylenedioxyisoquinoline (109741-34-6) + (+-)-bulbocapnine (72002-80-3)

Guidance literature:

With sulfuric acid; anschliessend mit Zink-Pulver und wss. HCl;

Downstream raw materials:

(S)-bulocapnine

Bulbocapnine methyl ether

Oxyhydrastinine

(S)-11-methoxy-7-methyl-12-(1-phenyl-1H-tetrazol-5-yloxy)-6,7,7a,8-tetrahydro-5H-benzo[g][1,3]dioxolo[4',5':4,5]benzo[1,2,3-de]quinoline

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