Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-

Base Information

Chemical Name:Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-
CAS No.:74051-60-8
Molecular Formula:C₁₈H₂₄N₄OS
Molecular Weight:344.481
Hs Code.:
DSSTox Substance ID:DTXSID60224967
Nikkaji Number:J127.563A
Wikidata:Q83103810
Mol file:74051-60-8.mol

Synonyms:74051-60-8;Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-;3-Antipyrinyl-1-cyclohexylthiourea;1-cyclohexyl-3-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)thiourea;BRN 0569078;1-Cyclohexyl-3-(4-antipyryl)-2-thiourea;3-(4-Antipyryl)-1-cyclohexyl-2-thiourea;1-cyclohexyl-3-(1,5-dimethyl-3-oxo-2-phenylpyrazol-4-yl)thiourea;Oprea1_659432;5-25-14-00108 (Beilstein Handbook Reference);DTXSID60224967;STK377075;AKOS002161879;SR-01000236454;SR-01000236454-1;F0856-0429

Suppliers and Price of Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-

Chemical Property:

Vapor Pressure:1.59E-08mmHg at 25°C
Boiling Point:456.7°Cat760mmHg
Flash Point:230°C
PSA：90.12000
Density:1.26g/cm³
LogP:3.58780
XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:344.16708258
Heavy Atom Count:24
Complexity:521

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=O)N(N1C)C2=CC=CC=C2)NC(=S)NC3CCCCC3

Technology Process of Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio-

There total 4 articles about Urea, 3-(4-antipyrinyl)-1-cyclohexyl-2-thio- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 1122-82-3
isothiocyanatocyclohexane

: 74051-60-8
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-N'-cyclohexylthiourea

Guidance literature:: In ethanol; for 1h; Heating;

Reference yield:

: 885-11-0
1,5-dimethyl-4-nitroso-2-phenyl-1,2-dihydro-pyrazol-3-one

: 74051-60-8
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-N'-cyclohexylthiourea

Guidance literature:: Multi-step reaction with 3 steps

1: Zn, glacial acetic acid / 1.) H₂O, C₂H₅OH; 2.) warming

2: 10percent HCl / 6 h / Heating

3: 90 percent / ethanol / 1 h / Heating

With hydrogenchloride; acetic acid; zinc; In ethanol;

Reference yield:

: 5702-68-1
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pryazol-4-yl)benzamide

: 74051-60-8
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-N'-cyclohexylthiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent HCl / 6 h / Heating

2: 90 percent / ethanol / 1 h / Heating

With hydrogenchloride; In ethanol;