3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-

Base Information

Chemical Name:3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-
CAS No.:3411-09-4
Molecular Formula:C17H24O3
Molecular Weight:276.376
Hs Code.:
Nikkaji Number:J109.669I
Wikidata:Q76305795
Mol file:3411-09-4.mol

Synonyms:3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-;3411-09-4;SCHEMBL20658114;XPWFZKSZSONJDK-MDZDMXLPSA-N;LS-154216;4-(2,6-Dimethoxy-4-pentylphenyl)-3-buten-2-one;(3E)-4-(2,6-Dimethoxy-4-pentylphenyl)-3-buten-2-one #

Suppliers and Price of 3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-

Chemical Property:

Vapor Pressure:3.46E-07mmHg at 25°C
Boiling Point:417.7°C at 760 mmHg
Flash Point:198.2°C
PSA：35.53000
Density:1.007g/cm³
LogP:4.03870
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:276.17254462
Heavy Atom Count:20
Complexity:297

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC1=CC(=C(C(=C1)OC)C=CC(=O)C)OC
Isomeric SMILES:CCCCCC1=CC(=C(C(=C1)OC)/C=C/C(=O)C)OC

Technology Process of 3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)-

There total 5 articles about 3-Buten-2-one, 4-(2,6-dimethoxy-4-pentylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3410-84-2
2,6-dimethoxy-4-pentylbenzaldehyde

: 67-64-1
acetone

: 3411-09-4
2.6-Dimethoxy-4-pentyl-benzalaceton

Guidance literature:: With sodium hydroxide; In water; at 60 ℃; for 12h;
DOI:10.1021/acs.orglett.7b03668

Reference yield: 80.0%

: 3410-84-2
2,6-dimethoxy-4-pentylbenzaldehyde

: 67-64-1
acetone

: 3411-09-4
(E)-4-(2,6-dimethoxy-4-pentylphenyl)but-3-en-2-one

Guidance literature:: With sodium hydroxide; In water; at 50 ℃; for 29h;
DOI:10.1021/jo100785w

Reference yield:

: 500-66-3
Olivetol

: 3411-09-4
2.6-Dimethoxy-4-pentyl-benzalaceton

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 12.08 h / 80 °C / Inert atmosphere

2.1: N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 1.67 h / -78 - 0 °C / Inert atmosphere

2.3: 1.53 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide / water / 12 h / 60 °C

With N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; acetone;
DOI:10.1021/acs.orglett.7b03668