O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate

Base Information

Chemical Name:O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate
CAS No.:71432-15-0
Molecular Formula:C₁₃H₁₁Cl₂O₂PS
Molecular Weight:333.175
Hs Code.:
DSSTox Substance ID:DTXSID70991810

Synonyms:O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate;71432-15-0;Phosphonothioic acid, phenyl-, O-(2,3-dichlorophenyl) O-methyl ester;BRN 2871610;Phenylphosphonothioic acid O-(2,3-dichlorophenyl) O-methyl ester;DTXSID70991810

Suppliers and Price of O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate

Chemical Property:

Vapor Pressure:2.02E-06mmHg at 25°C
Boiling Point:405.7°Cat760mmHg
Flash Point:199.1°C
Density:1.41g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:331.9594431
Heavy Atom Count:19
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COP(=S)(C1=CC=CC=C1)OC2=C(C(=CC=C2)Cl)Cl

Technology Process of O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate

There total 4 articles about O-(2,3-Dichlorophenyl) O-methyl phenylphosphonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.8%

: 67-56-1
methanol

: O-2,3-dichlorophenyl diethylamidophenylthiophosphonate

: 71432-15-0,95454-65-2,95454-66-3
O-methyl O-2,3-dichlorophenyl phenylthiophosphonate

Guidance literature:: With sulfuric acid; for 5h; Heating;
DOI:10.1007/BF00954118

Reference yield:

: 95454-60-7
sodium 2,3-dichlorophenoxide

: 71432-15-0,95454-65-2,95454-66-3
O-methyl O-2,3-dichlorophenyl phenylthiophosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92.7 percent / tetrahydrofuran / 48 h / 20 °C

2: 61.8 percent / aq. H₂SO₄ / 5 h / Heating

With sulfuric acid; In tetrahydrofuran;
DOI:10.1007/BF00954118

Reference yield:

: 5120-50-3
diethylamidophenylchlorothiophosphonate

: 71432-15-0,95454-65-2,95454-66-3
O-methyl O-2,3-dichlorophenyl phenylthiophosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92.7 percent / tetrahydrofuran / 48 h / 20 °C

2: 61.8 percent / aq. H₂SO₄ / 5 h / Heating

With sulfuric acid; In tetrahydrofuran;
DOI:10.1007/BF00954118