Methyl 2-iodo-4-nitrobenzoate

Base Information

Chemical Name:Methyl 2-iodo-4-nitrobenzoate
CAS No.:6326-42-7
Molecular Formula:C8H6INO4
Molecular Weight:307.044
Hs Code.:2916399090
NSC Number:30634
DSSTox Substance ID:DTXSID50283240
Wikidata:Q82017740
Mol file:6326-42-7.mol

Synonyms:methyl 2-iodo-4-nitrobenzoate;6326-42-7;2-Iodo-4-nitro-benzoic acid methyl ester;Benzoic acid, 2-iodo-4-nitro-, methyl ester;NSC30634;methyl2-iodo-4-nitrobenzoate;SCHEMBL1026910;DTXSID50283240;KRAIRAIRCFXHRZ-UHFFFAOYSA-N;MFCD00277928;NSC-30634;AKOS025287038;AS-47775;CS-0131379;F16107

Suppliers and Price of Methyl 2-iodo-4-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
Methyl 2-iodo-4-nitrobenzoate 95%
1 g
$ 104.00

SynQuest Laboratories
Methyl 2-iodo-4-nitrobenzoate 95%
5 g
$ 296.00

Crysdot
Methyl2-iodo-4-nitrobenzoate 95+%
10g
$ 2822.00

Crysdot
Methyl2-iodo-4-nitrobenzoate 95+%
5g
$ 1701.00

Chemcia Scientific
2-Iodo-4-nitro-benzoicacidmethylester 97%
10 G
$ 415.00

BLDpharm
Methyl2-iodo-4-nitrobenzoate 95%
5g
$ 1163.00

BLDpharm
Methyl2-iodo-4-nitrobenzoate 95%
1g
$ 317.00

BLDpharm
Methyl2-iodo-4-nitrobenzoate 95%
250mg
$ 158.00

Apolloscientific
Methyl2-iodo-4-nitrobenzoate 95%
1g
$ 95.00

Apolloscientific
Methyl2-iodo-4-nitrobenzoate 95%
5g
$ 269.00

Total 8 raw suppliers

Chemical Property of Methyl 2-iodo-4-nitrobenzoate

Chemical Property:

Vapor Pressure:2.37E-05mmHg at 25°C
Boiling Point:359.5°Cat760mmHg
Flash Point:171.2°C
PSA：72.12000
Density:1.904g/cm³
LogP:2.50920
Storage Temp.:2-8°C(protect from light)
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:306.93416
Heavy Atom Count:14
Complexity:240

Purity/Quality:

97% ^*data from raw suppliers

Methyl 2-iodo-4-nitrobenzoate 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=C(C=C(C=C1)[N+](=O)[O-])I

Technology Process of Methyl 2-iodo-4-nitrobenzoate

There total 4 articles about Methyl 2-iodo-4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 67-56-1
methanol

: 89459-38-1
4-nitro-2-iodobenzoic acid

: 6326-42-7
2-iodo-4-nitrobenzoic acid methyl ester

Guidance literature:: With sulfuric acid; for 20h; Heating;
DOI:10.1021/ol0270982

Reference yield:

: 3558-19-8
methyl 2-amino-4-nitrobenzoate

: 6326-42-7
2-iodo-4-nitrobenzoic acid methyl ester

Guidance literature:: methyl 2-amino-4-nitrobenzoate; With sulfuric acid; sodium nitrite; In water; at -10 - 0 ℃; for 2h;

With potassium iodide; In water; at -10 - 20 ℃; for 8h;

Reference yield:

: 619-17-0
4-Nitroanthranilic acid

: 6326-42-7
2-iodo-4-nitrobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / water / 1 h / 0 °C

1.2: 3 h / 0 °C

1.3: 20 h / 0 - 60 °C

2.1: sulfuric acid / water / 16 h / 85 °C

With sulfuric acid; In water;