[Amino(chloro)methylidene]azanium;chloride

Base Information

• Chemical Name: [Amino(chloro)methylidene]azanium;chloride
• CAS No.: 29671-92-9
• Molecular Formula: CH3 Cl N2 . Cl H
• Molecular Weight: 114.962
• Hs Code.: 2925290090
• Mol file: 29671-92-9.mol

Synonyms:

Chemical Property of [Amino(chloro)methylidene]azanium;chloride

Chemical Property:

• Vapor Pressure: 60.2mmHg at 25°C
• Melting Point: 180°C(lit.)
• Refractive Index: 1.6300 (estimate)
• Boiling Point: 88.8°Cat760mmHg
• Flash Point: 7.5°C
• PSA: 49.87000
• Density: 1.55g/cm³
• LogP: 1.72070
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 113.9751535
• Heavy Atom Count: 5
• Complexity: 27.5

Purity/Quality:

97% ^*data from raw suppliers

Chloroformamidine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=[NH2+])(N)Cl.[Cl-]

Technology Process of [Amino(chloro)methylidene]azanium;chloride

There total 4 articles about [Amino(chloro)methylidene]azanium;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

CYANAMID (420-04-2) → chloroformamidine hydrochloride (29671-92-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 2.5h;

DOI:10.1016/j.bmc.2006.03.001

Reference yield: 71.0%

Bis-(1-chloro-2,2-dimethyl-1-phenyl-propyl)-carbodiimide (71996-43-5) → 2,2-dimethylpropiophenone (938-16-9) + chloroformamidine hydrochloride (29671-92-9)

Guidance literature:

With water; In acetone; at 25 ℃; for 2h; Yields of byproduct given;

Reference yield: 65.0%

N,N'-bis(1-chloro-2,2,2-trifluoroethyl)carbodiimide (71996-41-3) → 2,2,2-Trifluoroacetophenone (434-45-7) + chloroformamidine hydrochloride (29671-92-9)

Guidance literature:

With water; In acetone; at 25 ℃; for 2h; Yields of byproduct given;

upstream raw materials:

CYANAMID

calcium cyanamide

Bis-(1-chloro-2,2-dimethyl-1-phenyl-propyl)-carbodiimide

N,N'-bis(1-chloro-2,2,2-trifluoroethyl)carbodiimide

Downstream raw materials:

5,6,7,8-tetrahydro-7-(benzyl)-pyrido[4',3':4,5]thieno[2,3-D]pyrimidin-2,4-diamine

7-phenyl-5,6,7,8-tetrahydro-benzo[4,5]thieno[2,3-d]pyrimidine-2,4-diamine

5-phenyl-5,6,7,8-tetrahydro-benzo[4,5]thieno[2,3-d]pyrimidine-2,4-diamine

5-(4-chloro-phenyl)-6-methyl-thieno[2,3-d]pyrimidine-2,4-diamine