U 48522A

Base Information

Chemical Name:U 48522A
CAS No.:65619-94-5
Molecular Formula:C₁₆H₂₃NO₃
Molecular Weight:277.364
Hs Code.:

Synonyms:

Suppliers and Price of U 48522A

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of U 48522A

Chemical Property:

Purity/Quality:

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Technology Process of U 48522A

There total 5 articles about U 48522A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 110-87-2
3,4-dihydro-2H-pyran

ethereal hydrogen chloride: ethereal hydrogen chloride

: 65619-92-3
8-(dimethylamino)-1,4-dioxaspiro-[4.5]-decane-8-carbonitrile

: 591-20-8
3-Bromophenol

: 65619-94-5
4-(m-hydroxyphenyl)-4-dimethylaminocyclohexanone ethylene ketal

Guidance literature:: With hydrogenchloride; sodium hydroxide; ammonium chloride; ammonia; sodium hydrogencarbonate; toluene-4-sulfonic acid; magnesium; In tetrahydrofuran; methanol; diethyl ether; chloroform; water; benzene;

Reference yield:

: 80165-54-4
Dimethyl-{8-[3-(tetrahydro-pyran-2-yloxy)-phenyl]-1,4-dioxa-spiro[4.5]dec-8-yl}-amine

: 65619-94-5
4-(m-hydroxyphenyl)-4-dimethylaminocyclohexanone ethylene ketal

Guidance literature:: With hydrogenchloride; Yield given;
DOI:10.1021/jm00135a019

Reference yield:

: 65619-92-3
8-(dimethylamino)-1,4-dioxaspiro-[4.5]-decane-8-carbonitrile

: 65619-94-5
4-(m-hydroxyphenyl)-4-dimethylaminocyclohexanone ethylene ketal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 2.) THF, reflux, 24 h

2: etheral HCl

With hydrogenchloride; magnesium;
DOI:10.1021/jm00135a019