N,N-dimethyl-P,P-diphenylphosphinic amide

Base Information

Chemical Name:N,N-dimethyl-P,P-diphenylphosphinic amide
CAS No.:3732-84-1
Molecular Formula:C14H16NOP
Molecular Weight:245.261
Hs Code.:
Mol file:3732-84-1.mol

Synonyms:

Suppliers and Price of N,N-dimethyl-P,P-diphenylphosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N,N-dimethyl-P,P-diphenylphosphinic amide

Chemical Property:

Vapor Pressure:3.41E-05mmHg at 25°C
Boiling Point:354.2°Cat760mmHg
Flash Point:168°C
Density:1.13g/cm³

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-dimethyl-P,P-diphenylphosphinic amide

There total 5 articles about N,N-dimethyl-P,P-diphenylphosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 16938-30-0
O-benzyl-N,N-dimethyl-hydroxylamine

: 4559-70-0
Diphenylphosphine oxide

: 3732-84-1
diphenylphosphinic acid dimethylamide

Guidance literature:: With potassium carbonate; In tert-Amyl alcohol; at 105 ℃; for 9h;
DOI:10.1021/acs.orglett.5b03056

Reference yield: 80.0%

: 124-40-3
dimethyl amine

: 4559-70-0
Diphenylphosphine oxide

: 3732-84-1
diphenylphosphinic acid dimethylamide

Guidance literature:: With tetrachloromethane; sodium hydroxide; In dichloromethane; water; at 0 - 25 ℃;
DOI:10.1007/s11172-009-0256-3

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 3732-84-1
diphenylphosphinic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water / benzene / 20 - 30 °C

1.2: pH 8 - 9

2.1: tetrachloromethane; sodium hydroxide / dichloromethane; water / 0 - 25 °C

With tetrachloromethane; water; sodium hydroxide; In dichloromethane; water; benzene; 2.1: Todd-Atherton reaction;
DOI:10.1007/s11172-009-0256-3