Hexahydrofuro[3,2-b]furan-3,6-diol

Base Information

Chemical Name:Hexahydrofuro[3,2-b]furan-3,6-diol
CAS No.:24332-71-6
Molecular Formula:C₆H₁₀O₄
Molecular Weight:146.143
Hs Code.:
European Community (EC) Number:248-906-7,211-374-1
NSC Number:270938,231906
DSSTox Substance ID:DTXSID801031676
Nikkaji Number:J250.678E
Mol file:24332-71-6.mol

Synonyms:1,4-3,6-dianhydro-D-mannitol;1,4-3,6-dianhydromannitol;isomannide

Suppliers and Price of Hexahydrofuro[3,2-b]furan-3,6-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 13 raw suppliers

Chemical Property of Hexahydrofuro[3,2-b]furan-3,6-diol

Chemical Property:

Boiling Point:372.1°Cat760mmHg
Flash Point:178.8°C
Density:1.475g/cm³
XLogP3:-1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:146.05790880
Heavy Atom Count:10
Complexity:122

Purity/Quality:: 99.5% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C2C(O1)C(CO2)O)O

Technology Process of Hexahydrofuro[3,2-b]furan-3,6-diol

There total 21 articles about Hexahydrofuro[3,2-b]furan-3,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3014-56-0,24332-64-7
(3S,3aR,6S,6aR)-6-(benzoyloxy)hexahydrofuro[3,2-b]furan-3-yl benzoate

: 641-74-7,652-67-5,5627-19-0,24332-71-6,28218-68-0,28948-16-5,28980-83-8,89825-36-5,124508-14-1,151380-60-8
1,4:3,6-dianhydro-L-iditol

Guidance literature:: With potassium cyanide; sodium methylate; In methanol; at 25 ℃; for 2h;
DOI:10.1016/S0957-4166(02)00411-1

Reference yield: 60.0%

: 50-70-4
D-sorbitol

: 616-38-6
carbonic acid dimethyl ester

: 641-74-7
1,4:3,6-dianhydro-D-mannitol

: 641-74-7,652-67-5,5627-19-0,24332-71-6,28218-68-0,28948-16-5,28980-83-8,89825-36-5,124508-14-1,151380-60-8
1,4:3,6-dianhydro-L-iditol

: 5306-85-4
isosorbide dimethyl ether

Guidance literature:: With triethylamine; In biphenyl; at 90 - 200 ℃; for 48h; under 63756.4 Torr; Reagent/catalyst; Autoclave; Inert atmosphere;
DOI:10.1002/cssc.201601382

Reference yield: 43.4%

: 641-74-7
1,4:3,6-dianhydro-D-mannitol

: 652-67-5
Isosorbide

: 641-74-7,652-67-5,5627-19-0,24332-71-6,28218-68-0,28948-16-5,28980-83-8,89825-36-5,124508-14-1,151380-60-8
1,4:3,6-dianhydro-L-iditol

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; 4,5-bis((diisopropylphosphanyl)methyl)acridine; In tert-Amyl alcohol; at 170 ℃; for 21h; Temperature; Inert atmosphere; Schlenk technique; Autoclave;
DOI:10.1002/cctc.201300407