diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

Base Information

Chemical Name:diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
CAS No.:10354-32-2
Molecular Formula:C21H27 N O6
Molecular Weight:389.448
Hs Code.:
Mol file:10354-32-2.mol

Synonyms:3,5-Pyridinedicarboxylicacid, 4-(3,4-dimethoxyphenyl)-1,4-dihydro-2,6-dimethyl-, diethyl ester(7CI,8CI,9CI);2,6-Dimethyl-3,5-bis(ethoxycarbonyl)-4-(3,4-dimethoxyphenyl)-1,4-dihydropyridine;DHP 51; Diethyl4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; NSC282463

Suppliers and Price of diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

Chemical Property:

Vapor Pressure:4.03E-10mmHg at 25°C
Boiling Point:499.8°Cat760mmHg
Flash Point:256°C
Density:1.14g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

There total 9 articles about diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 141-97-9
ethyl acetoacetate

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 10354-32-2
diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine 3,5-dicarboxylate

Guidance literature:: With ammonium acetate; Zn[(L)proline]2; In ethanol; for 0.0333333h; microwave irradiation;
DOI:10.1002/hc.20197

Reference yield: 90.0%

: 631-61-8,92206-38-7
ammonium acetate

: 141-97-9
ethyl acetoacetate

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 10354-32-2
diethyl 4-(3,4-dimethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine 3,5-dicarboxylate

Guidance literature:: ammonium acetate; ethyl acetoacetate; 3,4-dimethoxy-benzaldehyde; With cellulose sulfuric acid; In neat (no solvent); at 80 - 100 ℃;

With cellulose sulfuric acid; In neat (no solvent);
DOI:10.1016/j.bmcl.2012.05.003