Benzyl 2-phenylethyl ether

Base Information

• Chemical Name: Benzyl 2-phenylethyl ether
• CAS No.: 54894-37-0
• Molecular Formula: C15H16 O
• Molecular Weight: 212.291
• Hs Code.: 2909309090
• European Community (EC) Number: 259-386-6
• UNII: 9UP77D6TM4
• DSSTox Substance ID: DTXSID1068980
• Nikkaji Number: J326.700H
• Wikidata: Q81995757
• Mol file: 54894-37-0.mol

Synonyms:Benzyl 2-phenylethyl ether;54894-37-0;[(2-phenylethoxy)methyl]benzene;Benzene, ((2-phenylethoxy)methyl)-;9UP77D6TM4;((2-Phenylethoxy)methyl)benzene;EINECS 259-386-6;Benzene, [(2-phenylethoxy)methyl]-;Benzylphenethyl ether;UNII-9UP77D6TM4;SCHEMBL1066576;DTXSID1068980

Chemical Property of Benzyl 2-phenylethyl ether

Chemical Property:

• Vapor Pressure: 0.0017mmHg at 25°C
• Boiling Point: 303.1°C at 760 mmHg
• Flash Point: 145.8°C
• PSA: 9.23000
• Density: 1.031g/cm³
• LogP: 3.44590
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 212.120115130
• Heavy Atom Count: 16
• Complexity: 166

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CCOCC2=CC=CC=C2

Technology Process of Benzyl 2-phenylethyl ether

There total 39 articles about Benzyl 2-phenylethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-phenylethanol (60-12-8) + benzyl alcohol (100-51-6,185532-71-2) → (2-(benzyloxy)ethyl)benzene (54894-37-0)

Guidance literature:

With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I); at 150 ℃; for 0.5h; Kinetics; Inert atmosphere; Microwave irradiation;

DOI:10.1002/adsc.201401097

Reference yield: 95.0%

2-phenylethanol (60-12-8) + benzyl bromide (100-39-0) → (2-(benzyloxy)ethyl)benzene (54894-37-0)

Guidance literature:

2-phenylethanol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/jo801659g

Reference yield: 95.0%

benzyl P,P-diphenyl-N-(methanesulfonyl)phosphinimidate (864298-57-7) + 2-phenylethanol (60-12-8) → (2-(benzyloxy)ethyl)benzene (54894-37-0)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In 1,2-dimethoxyethane; at 20 ℃; for 1h;

DOI:10.1246/cl.2005.1016 DOI:10.1246/bcsj.79.1255

upstream raw materials:

sodium phenethylate

benzyl chloride

1-phenyl-2-bromoethane

benzyl alcohol

Downstream raw materials:

2-phenylethyl nitrite

phenylacetaldehyde

benzaldehyde

ethylbenzene