sodium alpha-hydroxy-p-methoxytoluene-alpha-sulphonate

Base Information

• Chemical Name: sodium alpha-hydroxy-p-methoxytoluene-alpha-sulphonate
• CAS No.: 33402-67-4
• Molecular Formula: C8H10 O5 S . Na
• Molecular Weight: 262.194
• Hs Code.: 2909499000
• Mol file: 33402-67-4.mol

Synonyms:Benzenemethanesulfonicacid, a-hydroxy-4-methoxy-, monosodiumsalt (9CI); a-Toluenesulfonicacid, a-hydroxy-p-methoxy-, monosodiumsalt (8CI); Anisaldehyde sodium bisulfite adduct; NSC 82331; Sodium a-hydroxy-4-methoxybenzenemethanesulfonate

Chemical Property of sodium alpha-hydroxy-p-methoxytoluene-alpha-sulphonate

Chemical Property:

• PSA: 92.21000
• LogP: 1.65470

Purity/Quality:

99% ^*data from raw suppliers

AnisaldehydeSodiumBisulfiteAdduct ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Anisaldehyde Sodium Bisulfite Adduct is an intermediate in the synthesis of Ambucetamide (A575935). Ambucetamide is an antispasmodic found to be particularly effective for the relief of menstrual pain.

Technology Process of sodium alpha-hydroxy-p-methoxytoluene-alpha-sulphonate

There total 4 articles about sodium alpha-hydroxy-p-methoxytoluene-alpha-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxy-benzaldehyde (123-11-5) → sodium hydroxy(4-methoxyphenyl)methanesulfonate (33402-67-4)

Guidance literature:

With sodium metabisulfite; In ethanol; at 4 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.ejmech.2020.112554

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → sodium hydroxy(4-methoxyphenyl)methanesulfonate (33402-67-4) + Sodium; (4-methoxy-phenyl)-sulfo-methanolate (33402-67-4) + C8H8O5S(2-)*2Na(1+) (33402-67-4)

Guidance literature:

With sodium metabisulfite; In water; at 25 ℃; Rate constant; pH=7;

DOI:10.1007/BF00901820

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → sodium hydroxy(4-methoxyphenyl)methanesulfonate (33402-67-4) + Sodium; (4-methoxy-phenyl)-sulfo-methanolate (33402-67-4) + C8H8O5S(2-)*2Na(1+) (33402-67-4)

Guidance literature:

With sodium metabisulfite; In water; at 25 ℃; Rate constant; pH=7;

DOI:10.1007/BF00901820

upstream raw materials:

4-methoxy-benzaldehyde

Downstream raw materials:

2-(4-methoxyphenyl)imidazo[1,2-a]pyridin-3-amine

5-chloro-2-(4-methoxyphenyl)-1H-benzo[d]imidazole

(E)-3-(4-methoxyphenyl)acrylic acid

trimethyl(4-methoxybenzyloxy)silane

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