Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide

Base Information

Chemical Name:Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide
CAS No.:54009-57-3
Molecular Formula:C10H12 N2 O2
Molecular Weight:192.217
Hs Code.:

Synonyms:Benzoicacid, 2-hydroxy-, (1-methylethylidene)hydrazide (9CI); Salicylic acid,isopropylidenehydrazide (6CI); Acetone salicyloylhydrazone; Isopropanonesalicyloylhydrazone; NSC 523269

Suppliers and Price of Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.14g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide

There total 1 articles about Benzoic acid,2-hydroxy-, 2-(1-methylethylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 936-02-7
2-Hydroxybenzoylhydrazine

: 67-64-1
acetone

: 54009-57-3
2-hydroxy-N'-(propan-2-ylidene)benzohydrazide

Guidance literature:: In methanol; for 0.5h; Heating;

Reference yield: 92.0%

: Co⁽²⁺⁾*2Cu⁽¹⁺⁾*4SCN^(1-) = Co[Cu(SCN)2]2

: 54009-57-3
2-hydroxy-N'-(propan-2-ylidene)benzohydrazide

: 2Cu⁽¹⁺⁾*Co⁽²⁺⁾*4NCS^(1-)*(C₆H₄(OH)CONHNC(CH₃)2)={CoCu₂(SCN)4(C₆H₄(OH)CONHNC(CH₃)2)}

Guidance literature:: In 1,4-dioxane; hexane; suspending CoCu2(SCN)4 in dry hexane (separately); stirring with in dioxane dissolved hydrazone for 30-75h at room temp. (till apparent color change);; filtration through a closed assembly; washing with dioxane/hexane; drying in a vac. desiccator at room temp.; elem. anal.;;

Reference yield: 91.0%

: (copper(II) tetrathiocyanatodiargentate(I))n

: 54009-57-3
2-hydroxy-N'-(propan-2-ylidene)benzohydrazide

: (copper(II) tetrathiocyanatoargentate(I)*isopropanone salicyloylhydrazone)n

Guidance literature:: In 1,4-dioxane; suspending CuAg2(SCN)4 in dioxane, mixing with ligand in dioxane, stirring for 25-65 h; filtn., washing with dioxane, drying in a desiccator at room temp., elem. anal.;