1-Ethyl-1,2,5,6-tetrahydropyridine

Base Information

• Chemical Name: 1-Ethyl-1,2,5,6-tetrahydropyridine
• CAS No.: 6972-40-3
• Molecular Formula: C7H13N
• Molecular Weight: 111.187
• Mol file: 6972-40-3.mol

Synonyms:1-Aethyl-1,2,3,6-tetrahydro-pyridin;1-Ethyl-1,2,3,6-tetrahydropyridine;N-ETHYL-1,2,5,6-TETRAHYDROPYRIDINE;1-ethyl-1,2,5,6-tetrahydropyridine;

Chemical Property of 1-Ethyl-1,2,5,6-tetrahydropyridine

Chemical Property:

• Vapor Pressure: 5.84mmHg at 25°C
• Boiling Point: 141.5°Cat760mmHg
• Flash Point: 31.4°C
• PSA: 3.24000
• Density: 0.866g/cm³
• LogP: 1.20610

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Ethyl-1,2,5,6-tetrahydropyridine

There total 12 articles about 1-Ethyl-1,2,5,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-(2-phenylselenoethyl)-1,2,5,6-tetrahydropyridine → 1-ethyl-1,2,5,6-tetrahydropyridine (6972-40-3)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 3h; Heating;

DOI:10.1021/jo000790v

Reference yield:

→ 1-ethyl-piperidine (766-09-6) + 1-ethyl-1,2,5,6-tetrahydropyridine (6972-40-3)

Guidance literature:

With formic acid; potassium formate; at 160 ℃;

Reference yield:

N-ethylpiperidin-4-yl acetate (850452-52-7) → 1-ethyl-1,2,5,6-tetrahydropyridine (6972-40-3)

Guidance literature:

With 4-tert-Butylcatechol; at 485 ℃;

DOI:10.1021/ja01639a052

upstream raw materials:

pyridine

ethyl bromide

1-Aethyl-4-chlor-piperidin

N-ethylpiperidin-4-yl acetate