N-bis(phenylmethoxy)phosphorylaniline

Base Information

Chemical Name:N-bis(phenylmethoxy)phosphorylaniline
CAS No.:56883-96-6
Molecular Formula:C20H20NO3P
Molecular Weight:353.3515
Hs Code.:
NSC Number:122784
DSSTox Substance ID:DTXSID50298379
Wikidata:Q82040162

Synonyms:56883-96-6;N-bis(phenylmethoxy)phosphorylaniline;Dibenzyl anilinophosphonate;Dibenzyl phenylamidophosphate #;DTXSID50298379;QHAMRRYRTCVVSF-UHFFFAOYSA-N;NSC122784;NSC-122784

Suppliers and Price of N-bis(phenylmethoxy)phosphorylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-bis(phenylmethoxy)phosphorylaniline

Chemical Property:

Vapor Pressure:1.6E-09mmHg at 25°C
Boiling Point:484°Cat760mmHg
Flash Point:246.5°C
Density:1.245g/cm³
XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:353.11808050
Heavy Atom Count:25
Complexity:387

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COP(=O)(NC2=CC=CC=C2)OCC3=CC=CC=C3

Technology Process of N-bis(phenylmethoxy)phosphorylaniline

There total 8 articles about N-bis(phenylmethoxy)phosphorylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 62-53-3
aniline

: 220185-51-3
dibenzyl bromophosphate

: 56883-96-6
dibenzyl N-phenylphosphoramidate

Guidance literature:: In dichloromethane; at -30 - 20 ℃; for 2h;
DOI:10.1021/jo010495q

Reference yield: 63.0%

: 17176-77-1
Dibenzyl phosphite

: 62-53-3
aniline

: 56883-96-6
dibenzyl N-phenylphosphoramidate

Guidance literature:: With tetrachloromethane; tetrabutylammomium bromide; potassium carbonate; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1080/10426500500536614

Reference yield:

: 15205-57-9
tribenzyl phosphite

: 56883-96-6
dibenzyl N-phenylphosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / CH₂Cl₂ / 0.42 h / 0 - 20 °C

2: 97 percent / CH₂Cl₂ / 2 h / -30 - 20 °C

With bromine; In dichloromethane;
DOI:10.1021/jo010495q