1-Phenyl-1,2-butanediol

Base Information

Chemical Name:1-Phenyl-1,2-butanediol
CAS No.:22607-13-2
Molecular Formula:C10H14 O2
Molecular Weight:166.22
Hs Code.:2906299090
DSSTox Substance ID:DTXSID40945264
Nikkaji Number:J129.331A
Mol file:22607-13-2.mol

Synonyms:1-phenylbutane-1,2-diol;1-Phenyl-1,2-butanediol;22607-13-2;1,2-Butanediol, 1-phenyl-;1-Phenyl-1,2-butanediol #;SCHEMBL6939841;DTXSID40945264;WFSOUGZEVPHHSM-UHFFFAOYSA-N

Suppliers and Price of 1-Phenyl-1,2-butanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Phenyl-1,2-butanediol

Chemical Property:

Vapor Pressure:0.000306mmHg at 25°C
Boiling Point:307.8°Cat760mmHg
Flash Point:148.8°C
PSA：40.46000
Density:1.097g/cm³
LogP:1.49090
XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:166.099379685
Heavy Atom Count:12
Complexity:119

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C(C1=CC=CC=C1)O)O

Technology Process of 1-Phenyl-1,2-butanediol

There total 10 articles about 1-Phenyl-1,2-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 73951-65-2
trans-2-ethyl-3-phenyl-oxirane

: 22607-13-2
1-phenylbutane-1,2-diol

Guidance literature:: With sulfuric acid; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1002/anie.200601574

Reference yield: 42.0%

: 71-23-8
propan-1-ol

: 100-52-7
benzaldehyde

: 492-70-6,655-48-1,2325-10-2,38270-73-4,52340-78-0,579-43-1
1,2-diphenyl-1,2-ethanediol

: 22607-13-2
1-phenylbutane-1,2-diol

Guidance literature:: at 20 ℃; for 10h;
DOI:10.1016/S0040-4039(99)01357-X

Reference yield:

: 21087-29-6
trans-3-phenylprop-2-enyl chloride

: 22607-13-2
1-phenylbutane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper iodide / diethyl ether / 1 h / 20 °C

1.2: 37 percent / diethyl ether / 18 h / 20 °C

2.1: 77 percent / m-chloroperoxybenzoic acid; Na₂HPO₄ / CH₂Cl₂ / 3.5 h / 0 - 20 °C

3.1: 95 percent / H₂SO₄ / H₂O; tetrahydrofuran / 20 °C

With disodium hydrogenphosphate; copper(l) iodide; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1002/anie.200601574