2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)

Base Information

Chemical Name:2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)
CAS No.:86745-99-5
Molecular Formula:C₁₆H₂₅BrN₂O₂*ClH
Molecular Weight:393.752
Hs Code.:
DSSTox Substance ID:DTXSID501007072

Synonyms:86745-99-5;DTXSID501007072;2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)

Suppliers and Price of 2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)

Chemical Property:

Vapor Pressure:4.61E-10mmHg at 25°C
Boiling Point:498.2°Cat760mmHg
Flash Point:255.1°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:392.08662
Heavy Atom Count:22
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCNC(=O)COC1=CC(=C(C(=C1)C)Br)C.Cl

Technology Process of 2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1)

There total 3 articles about 2-(4-Bromo-3,5-dimethylphenoxy)-N-[2-(diethylamino)ethyl]ethanimidic acid--hydrogen chloride (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 86745-93-9
(4-bromo-3,5-dimethylphenoxy)acetic acid methyl ester

: 100-36-7
N,N-diethylethylenediamine

: 86745-99-5
2-(4-Bromo-3,5-dimethyl-phenoxy)-N-(2-diethylamino-ethyl)-acetamide; hydrochloride

Guidance literature:: With hydrogenchloride; 1.) ethanol, reflux 20 h, 2.) ether;
DOI:10.1135/cccc19831089

Reference yield:

: 7463-51-6
4-bromo-3,5-dimethylphenol

: 86745-99-5
2-(4-Bromo-3,5-dimethyl-phenoxy)-N-(2-diethylamino-ethyl)-acetamide; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaOH / H₂O / 1.) 90 deg C, 1 h, 2.) 4 h.

2: 58 percent / methanol / 10 h / Heating

3: 82 percent / HCl / 1.) ethanol, reflux 20 h, 2.) ether

With hydrogenchloride; sodium hydroxide; In methanol; water;
DOI:10.1135/cccc19831089

Reference yield:

: 86745-92-8
sodium 4-bromo-3,5-dimethylphenoxyacetate

: 86745-99-5
2-(4-Bromo-3,5-dimethyl-phenoxy)-N-(2-diethylamino-ethyl)-acetamide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / methanol / 10 h / Heating

2: 82 percent / HCl / 1.) ethanol, reflux 20 h, 2.) ether

With hydrogenchloride; In methanol;
DOI:10.1135/cccc19831089