Benzyl β-D-ribopyranoside tribenzoate

Base Information

• Chemical Name: Benzyl β-D-ribopyranoside tribenzoate
• CAS No.: 13035-46-6
• Molecular Formula: C₃₃H₂₈O₈
• Molecular Weight: 552.581
• Hs Code.: 2932999099
• Mol file: 13035-46-6.mol

Synonyms:Ribopyranoside,benzyl, tribenzoate (7CI); Ribopyranoside, benzyl, tribenzoate, b-D- (8CI); NSC 231858

Chemical Property of Benzyl β-D-ribopyranoside tribenzoate

Chemical Property:

• Vapor Pressure: 1.17E-18mmHg at 25°C
• Boiling Point: 685.7°Cat760mmHg
• Flash Point: 287.4°C
• PSA: 97.36000
• Density: 1.31g/cm³
• LogP: 5.23630

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzyl β-D-ribopyranoside tribenzoate

There total 3 articles about Benzyl β-D-ribopyranoside tribenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O2,O3,O4-Tribenzoyl-β-D-ribopyranose (909273-47-8) → benzyl-(tri-O-benzoyl-β-D-ribopyranoside) (13035-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane; hydrogen bromide; acetic acid / Zusatz von Acetanhydrid

With hydrogen bromide; acetic acid; 1,2-dichloro-ethane;

DOI:10.1021/ja01632a037

Reference yield:

benzoyl chloride (98-88-4) + benzyl-β-D-ribopyranoside (70797-93-2) → benzyl-(tri-O-benzoyl-β-D-ribopyranoside) (13035-46-6)

Guidance literature:

With pyridine;

DOI:10.1021/ja01632a037

Reference yield:

benzyl alcohol (100-51-6,185532-71-2) + 2,3,4-tri-O-benzoyl-β-D-ribopyranosyl bromide (13035-44-4,13035-48-8,14206-56-5,14262-83-0,40010-17-1,50271-21-1,58407-63-9,60426-89-3,90365-68-7,108508-31-2,108942-37-6,145374-03-4) → benzyl-(tri-O-benzoyl-β-D-ribopyranoside) (13035-46-6)

Guidance literature:

DOI:10.1021/ja01632a037

upstream raw materials:

benzoyl chloride

benzyl-β-D-ribopyranoside

benzyl alcohol

2,3,4-tri-O-benzoyl-β-D-ribopyranosyl bromide

Downstream raw materials:

O²,O³,O⁴-Tribenzoyl-β-D-ribopyranose