4-(Chloromethyl)-2-phenyl-1,3-dioxolane

Base Information

Chemical Name:4-(Chloromethyl)-2-phenyl-1,3-dioxolane
CAS No.:36236-72-3
Molecular Formula:C10H11ClO2
Molecular Weight:198.649
Hs Code.:
NSC Number:41981
DSSTox Substance ID:DTXSID00957626
Nikkaji Number:J83.702D
Mol file:36236-72-3.mol

Synonyms:4-(chloromethyl)-2-phenyl-1,3-dioxolane;36236-72-3;4-Chloromethyl-2-phenyl-1,3-dioxolane;NSC 41981;AI3-31949;1,3-DIOXOLANE, 4-CHLOROMETHYL-2-PHENYL-;1,3-Dioxolane, 4-(chloromethyl)-2-phenyl-;NSC41981;4-CHLOROMETHYL-2-PHENYL1,3-DIOXOLANE-;SCHEMBL15157163;DTXSID00957626;1, 4-(chloromethyl)-2-phenyl-;BBL029459;NSC-41981;STK802076;AKOS006277948;2-phenyl-4-chloromethyl-1,3-dioxolane;LS-62522;VS-09246;4-(chloromethyl)-2-phenyl-1,3-diox-olane;CS-0256491;EN300-6491862

Suppliers and Price of 4-(Chloromethyl)-2-phenyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
4-(Chloromethyl)-2-phenyl-1,3-dioxolane
100mg
$ 203.00

Total 7 raw suppliers

Chemical Property of 4-(Chloromethyl)-2-phenyl-1,3-dioxolane

Chemical Property:

Vapor Pressure:0.00225mmHg at 25°C
Boiling Point:298.5°Cat760mmHg
Flash Point:124.7°C
PSA：18.46000
Density:1.186g/cm³
LogP:2.33940
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:198.0447573
Heavy Atom Count:13
Complexity:157

Purity/Quality:

99% ^*data from raw suppliers

4-(Chloromethyl)-2-phenyl-1,3-dioxolane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(OC(O1)C2=CC=CC=C2)CCl

Technology Process of 4-(Chloromethyl)-2-phenyl-1,3-dioxolane

There total 9 articles about 4-(Chloromethyl)-2-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100-52-7
benzaldehyde

: 96-24-2
3-monochloro-1,2-propanediol

: 36236-72-3
4-chloromethyl-2-phenyl[1,3]dioxolane

Guidance literature:: With FIBAN K-1 cation exchanger; In benzene; Dean-Stark; Reflux;
DOI:10.1134/S1070363212090149

Reference yield: 72.0%

: 100-52-7
benzaldehyde

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 36236-72-3
4-chloromethyl-2-phenyl[1,3]dioxolane

Guidance literature:: tetrafluoroboric acid; In water; at 160 ℃; for 2h;
DOI:10.1007/BF00633210

Reference yield:

: 7527-52-8
2-phenyl-1,3-benzodioxole

: 36236-72-3
4-chloromethyl-2-phenyl[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) iodine monochloride, 2.) aq. Na₂S₂O₃ / 1.) 1 h, room temperature

2: 42 g / anhydrous tin(IV) chloride / CHCl₃ / 48 h / Ambient temperature

With Iodine monochloride; tin(IV) chloride; sodium thiosulfate; In chloroform;
DOI:10.1039/P19810000977