1-Methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine

Base Information

• Chemical Name: 1-Methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine
• CAS No.: 66706-33-0
• Molecular Formula: C₁₃H₁₁N₅O₆
• Molecular Weight: 333.26
• NSC Number: 156552
• DSSTox Substance ID: DTXSID40303082
• Nikkaji Number: J2.812.291H
• Wikidata: Q82048196

Synonyms:66706-33-0;1-methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine;NSC156552;DTXSID40303082;NSC-156552

Chemical Property of 1-Methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine

Chemical Property:

• Vapor Pressure: 1.86E-08mmHg at 25°C
• Boiling Point: 454.7°Cat760mmHg
• Flash Point: 228.8°C
• Density: 1.584g/cm³
• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 3
• Exact Mass: 333.07093309
• Heavy Atom Count: 24
• Complexity: 457

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C1=CC=CC=C1)NC2=C(C=C(C=C2[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1-Methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine

There total 4 articles about 1-Methyl-1-phenyl-2-(2,4,6-trinitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

pyridinium picrate (1152-90-5) + 1-Methyl-1-phenylhydrazine (618-40-6) → N-methyl-N-phenyl-N'-picryl-hydrazine (66706-33-0)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; water; for 0.5h; Heating in water bath;

DOI:10.1016/j.saa.2009.10.045

Reference yield:

1-methoxy-2,4,6-trinitrobenzene (606-35-9) + 1-Methyl-1-phenylhydrazine (618-40-6) → N-methyl-N-phenyl-N'-picryl-hydrazine (66706-33-0)

Guidance literature:

With ethanol; at 45 ℃;

Reference yield:

N-methyl-N-nitrosoaniline (614-00-6) → N-methyl-N-phenyl-N'-picryl-hydrazine (66706-33-0)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

With lithium aluminium tetrahydride;

DOI:10.1021/jo01372a023

upstream raw materials:

1-methoxy-2,4,6-trinitrobenzene

1-Methyl-1-phenylhydrazine

naphthalene; compound with 2-chloro-1,3,5-trinitro-benzene

N-methyl-N-nitrosoaniline

Downstream raw materials:

N'-methyl-N'-phenyl-N-picryl-hydrazine

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