4-methyl-6-[1-[2-[1-(3-methyl-6-oxo-1-cyclohexa-2,4-dienylidene)ethyla mino]ethylamino]ethylidene]cyclohexa-2,4-dien-1-one

Base Information

• Chemical Name: 4-methyl-6-[1-[2-[1-(3-methyl-6-oxo-1-cyclohexa-2,4-dienylidene)ethyla mino]ethylamino]ethylidene]cyclohexa-2,4-dien-1-one
• CAS No.: 60630-08-2
• Molecular Formula: C₂₀H₂₄N₂O₂
• Molecular Weight: 324.423
• Mol file: 60630-08-2.mol

Synonyms:NSC 362150

Chemical Property of 4-methyl-6-[1-[2-[1-(3-methyl-6-oxo-1-cyclohexa-2,4-dienylidene)ethyla mino]ethylamino]ethylidene]cyclohexa-2,4-dien-1-one

Chemical Property:

• Boiling Point: 514.1oC at 760 mmHg
• Flash Point: 170.6oC
• PSA: 65.18000
• Density: 1.126g/cm3
• LogP: 4.03280

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methyl-6-[1-[2-[1-(3-methyl-6-oxo-1-cyclohexa-2,4-dienylidene)ethyla mino]ethylamino]ethylidene]cyclohexa-2,4-dien-1-one

There total 6 articles about 4-methyl-6-[1-[2-[1-(3-methyl-6-oxo-1-cyclohexa-2,4-dienylidene)ethyla mino]ethylamino]ethylidene]cyclohexa-2,4-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

6-Methyl-4-oxo-4H-1-benzopyran-2-carboxylic acid (5006-44-0) + ethylenediamine (107-15-3,85404-18-8) → N,N'-bis-<1-(2-hydroxy-5-methylphenyl)ethylidene>ethylenediamine (60630-08-2) + 5-(2-hydroxy-5-methylphenyl)-2,3-dihydro-1,4-diazepine-7-carboxylic acid (90380-28-2)

Guidance literature:

at 80 - 110 ℃; for 4h;

Reference yield: 46.0%

5-(2-hydroxy-5-methylphenyl)-2,3-dihydro-1,4-diazepine-7-carboxylic acid (90380-28-2) → N,N'-bis-<1-(2-hydroxy-5-methylphenyl)ethylidene>ethylenediamine (60630-08-2)

Guidance literature:

With ethylenediamine;

Reference yield: 31.0%

6-methyl-chromen-4-one (38445-23-7) + ethylenediamine (107-15-3,85404-18-8) → N,N'-bis-<1-(2-hydroxy-5-methylphenyl)ethylidene>ethylenediamine (60630-08-2) + 5-(2-hydroxy-5-methylphenyl)-2,3-dihydro-1,4-diazepine (90380-32-8)

Guidance literature:

for 48h;

upstream raw materials:

5-methyl-2-hydroxyacetophenone

ethylenediamine

6-methyl-chromen-4-one

6-Methyl-4-oxo-4H-1-benzopyran-2-carboxylic acid

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