Technology Process of Tris(2-methylprop-2-en-1-yl) borate
There total 4 articles about Tris(2-methylprop-2-en-1-yl) borate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
benzene;
byproducts: ethanol; exclusion of moisture; a mixt. of metal alkoxide and methallyl alcohol in dry benzene was refluxed with fractional sepn. of alcohol/benzene azeotrope;; removal of solvent under reduced pressure; distn. (vac.); elem. anal.;;
- Guidance literature:
-
In
benzene;
exclusion of moisture; a mixt. of B2O3 and HOCH2C(CH3)CH2 in dry benzene was refluxed with fractional sepn. of the formed H2O;; removal of solvent under reduced pressure; distn. (vac.); elem. anal.;;
- Guidance literature:
-
In
neat (no solvent);
exclusion of moisture; disproportionation by heating of alkenoxy boroxine to 100-135°C/1.0 mmHg (a much higher temp. then b.p. of corresponding orthoborate);
