4-Amino-2-methoxyoxane-3,5-diol

Base Information

Chemical Name:4-Amino-2-methoxyoxane-3,5-diol
CAS No.:28412-78-4
Molecular Formula:C6H13 N O4
Molecular Weight:163.174
Hs Code.:
NSC Number:109169,104536
DSSTox Substance ID:DTXSID40295716
Mol file:28412-78-4.mol

Synonyms:4-amino-2-methoxyoxane-3,5-diol;113564-71-9;Pentopyranoside, methyl 3-amino-3-deoxy- (6CI);28412-78-4;methyl 3-amino-3-deoxypentopyranoside;NSC104536;DTXSID40295716;NSC109169;NSC-104536;NSC-109169

Suppliers and Price of 4-Amino-2-methoxyoxane-3,5-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4-Amino-2-methoxyoxane-3,5-diol

Chemical Property:

Vapor Pressure:6.3E-06mmHg at 25°C
Boiling Point:339.1°Cat760mmHg
Flash Point:158.9°C
Density:1.32g/cm³
XLogP3:-2.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:163.08445790
Heavy Atom Count:11
Complexity:132

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1C(C(C(CO1)O)N)O

Technology Process of 4-Amino-2-methoxyoxane-3,5-diol

There total 15 articles about 4-Amino-2-methoxyoxane-3,5-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 92051-08-6
methyl-3-desoxy-3-(dibenzyl)amino-α-D,L-lyxopyranoside

: 28412-78-4,28412-79-5,92051-09-7,112791-22-7,113532-34-6,113564-71-9,122291-83-2,122291-84-3,124439-55-0,124439-56-1,128583-65-3
methyl-3-amino-3-desoxy-α-D,L-lyxopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 16h;
DOI:10.1016/0008-6215(84)85335-5

Reference yield:

: 75754-41-5
4-desoxy-1,2-O-isopropylidene-β-D,L-threo-pentopyranose

: 28412-78-4,28412-79-5,92051-09-7,112791-22-7,113532-34-6,113564-71-9,122291-83-2,122291-84-3,124439-55-0,124439-56-1,128583-65-3
methyl-3-amino-3-desoxy-α-D,L-lyxopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / pyridinium chlorochromate / CH₂Cl₂ / 16 h

2: 70 percent / molecular sieves 3A / benzene / 24 h

3: 1.) B₂H₆; 2.) H₂O₂,NaOH / 2.) Pd/C / 1.) THF, 48 h, r.t.; 2.) 2.5 h, reflux; 2 h, r.t., ethanol

4: 70 percent / HCl / 2 h / Ambient temperature

5: 100 percent / H₂ / Pd/C / methanol / 16 h

With hydrogenchloride; sodium hydroxide; 3 A molecular sieve; hydrogen; dihydrogen peroxide; pyridinium chlorochromate; diborane; palladium on activated charcoal; In methanol; dichloromethane; benzene;
DOI:10.1016/0008-6215(84)85335-5

Reference yield:

: 75754-45-9
4-desoxy-1,2-O-isopropylidene-α-D,L-glycero-pentopyranos-3-ulose

: 28412-78-4,28412-79-5,92051-09-7,112791-22-7,113532-34-6,113564-71-9,122291-83-2,122291-84-3,124439-55-0,124439-56-1,128583-65-3
methyl-3-amino-3-desoxy-α-D,L-lyxopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / molecular sieves 3A / benzene / 24 h

2: 1.) B₂H₆; 2.) H₂O₂,NaOH / 2.) Pd/C / 1.) THF, 48 h, r.t.; 2.) 2.5 h, reflux; 2 h, r.t., ethanol

3: 70 percent / HCl / 2 h / Ambient temperature

4: 100 percent / H₂ / Pd/C / methanol / 16 h

With hydrogenchloride; sodium hydroxide; 3 A molecular sieve; hydrogen; dihydrogen peroxide; diborane; palladium on activated charcoal; In methanol; benzene;
DOI:10.1016/0008-6215(84)85335-5