Phenol, m-(methylnitrosamino)-

Base Information

Chemical Name:Phenol, m-(methylnitrosamino)-
CAS No.:23040-64-4
Molecular Formula:C₇H₈N₂O₂
Molecular Weight:152.153
Hs Code.:
DSSTox Substance ID:DTXSID30177597
Nikkaji Number:J86.610E
Wikidata:Q83047910
ChEMBL ID:CHEMBL156668

Synonyms:Phenol, m-(methylnitrosamino)-;CHEMBL156668;23040-64-4;m-(Methylnitrosamino)phenol;BRN 2965075;DTXSID30177597;BDBM50214513

Suppliers and Price of Phenol, m-(methylnitrosamino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phenol, m-(methylnitrosamino)-

Chemical Property:

Vapor Pressure:1.33E-05mmHg at 25°C
Boiling Point:357.4°C at 760 mmHg
Flash Point:170°C
Density:1.2g/cm³
XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:152.058577502
Heavy Atom Count:11
Complexity:140

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC(=CC=C1)O)N=O

Technology Process of Phenol, m-(methylnitrosamino)-

There total 6 articles about Phenol, m-(methylnitrosamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14703-69-6
3-(N-methylamino)phenol

: 23040-64-4
3-hydroxy-N-methyl-N-nitrosoaniline

Guidance literature:: With hydrogenchloride; sodium nitrite; In tetrahydrofuran;
DOI:10.7164/antibiotics.48.1460

Reference yield:

: 121942-75-4
3-[(tert-butyldimethylsilyl)oxy]aniline

: 23040-64-4
3-hydroxy-N-methyl-N-nitrosoaniline

Guidance literature:: Multi-step reaction with 4 steps

1: Py / CH₂Cl₂

2: NaH / dimethylformamide

3: aq. K₂CO₃ / methanol

4: aq. NaNO₂, HCl / tetrahydrofuran

With pyridine; hydrogenchloride; sodium hydride; potassium carbonate; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.48.1460

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 23040-64-4
3-hydroxy-N-methyl-N-nitrosoaniline

Guidance literature:: Multi-step reaction with 5 steps

1: imidazole / dimethylformamide

2: Py / CH₂Cl₂

3: NaH / dimethylformamide

4: aq. K₂CO₃ / methanol

5: aq. NaNO₂, HCl / tetrahydrofuran

With pyridine; 1H-imidazole; hydrogenchloride; sodium hydride; potassium carbonate; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.48.1460