N,N-diethylcarbamodithioate;dioxomolybdenum(2+)

Base Information

Chemical Name:N,N-diethylcarbamodithioate;dioxomolybdenum(2+)
CAS No.:19680-83-2
Molecular Formula:C₁₀H₂₀MoN₂O₂S₄
Molecular Weight:424.485
Hs Code.:
European Community (EC) Number:631-550-5
Mol file:19680-83-2.mol

Synonyms:N,N-diethylcarbamodithioate;dioxomolybdenum(2+);19680-83-2;Bis(diethyldithiocarbamato)dioxomolybdenum(VI);MoO2(S2CNEt2)2;Molybdenum, bis(diethylcarbamodithioato-S,S')dioxo-

Suppliers and Price of N,N-diethylcarbamodithioate;dioxomolybdenum(2+)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of N,N-diethylcarbamodithioate;dioxomolybdenum(2+)

Chemical Property:

Vapor Pressure:1.1mmHg at 25°C
Melting Point:103°C (dec.)
Boiling Point:176.4°C at 760 mmHg
Flash Point:60.5°C
PSA：155.40000
LogP:3.38360
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:425.946166
Heavy Atom Count:19
Complexity:251

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 36/37/38-20/21/22
Safety Statements: 26-36/37/39-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=S)[S-].CCN(CC)C(=S)[S-].O=[Mo+2]=O

Technology Process of N,N-diethylcarbamodithioate;dioxomolybdenum(2+)

There total 9 articles about N,N-diethylcarbamodithioate;dioxomolybdenum(2+) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: hexaammonium heptamolybdate tetrahydrate

: 20624-25-3
sodium diethyldithiocarbamate trihydrate

: 19680-83-2
bis(N,N-diethyldithiocarbamato)dioxomolybdenum(VI)

Guidance literature:: With HNO₃; In water; a soln. of Na comp. slowly added to a soln. of molybdate with strong stirring, pH kepted at about 2 (1 M HNO3); ppt. filtered, washed (water), dried (vac.), recrystd. (benzene:hexane 1:1); elem. anal.;
DOI:10.1016/S0277-5387(00)00496-4

Reference yield: 85.0%

: sodium molybdate

: 148-18-5
sodium N,N-diethyldithiocarbamate

: 19680-83-2
bis(N,N-diethyldithiocarbamato)dioxomolybdenum(VI)

Guidance literature:: With hydrogenchloride; In water; for 2h;

Reference yield: 67.0%

: 7631-95-0
sodium molybdate dihydrate

: 20624-25-3
sodium diethyldithiocarbamate trihydrate

: 19680-83-2
bis(N,N-diethyldithiocarbamato)dioxomolybdenum(VI)

Guidance literature:: With hydrogenchloride; In water; according to: F. W. Moore and M. L. Larson, Inorg. Chem. 1967, 6, 998., adding HCl; filtn., washing (H2O), drying, recrystallization (Et2O, benzene);
DOI:10.1016/0277-5387(95)00217-G