Methyl 3-hydroxy-1-benzofuran-2-carboxylate

Base Information

• Chemical Name: Methyl 3-hydroxy-1-benzofuran-2-carboxylate
• CAS No.: 5117-55-5
• Molecular Formula: C10H8O4
• Molecular Weight: 192.171
• Hs Code.: 2932999099
• Mol file: 5117-55-5.mol

Synonyms:methyl 3-hydroxybenzofuran-2-carboxylate;3-hydroxy-benzofuran-2-carboxylic acid methyl ester;methyl 3-hydroxybenzofuran-2-carboxylate;3-Hydroxy-cumarilsaeure-methylester;HMS1629L13;3-Hydroxy-benzofuran-2-carbonsaeure-methylester;methyl 3-hydroxy-2-benzofurancarboxylate;2-Carbomethoxy-3-hydroxy-benzofuran;

Chemical Property of Methyl 3-hydroxy-1-benzofuran-2-carboxylate

Chemical Property:

• Vapor Pressure: 0.00124mmHg at 25°C
• Boiling Point: 432.2°Cat760mmHg
• PKA: 7.09±0.50(Predicted)
• Flash Point: 161.4°C
• PSA: 59.67000
• Density: 1.306g/cm³
• LogP: 1.92500

Purity/Quality:

97% ^*data from raw suppliers

Methyl3-hydroxybenzofuran-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 3-hydroxy-1-benzofuran-2-carboxylate

There total 1 articles about Methyl 3-hydroxy-1-benzofuran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

methyl <(2-methoxycarbonyl)phenoxy>acetate (56424-76-1) → methyl 3-hydroxybenzofuran-2-carboxylate (5117-55-5) + (2-carboxyphenoxy)acetic acid (635-53-0)

Guidance literature:

With potassium hydroxide; cetyltrimethylammonim bromide; In toluene; at 110 ℃; for 2h;

DOI:10.1135/cccc19930592

Reference yield: 69.0%

methyl 3-hydroxybenzofuran-2-carboxylate (5117-55-5) + 2,2-dimethyl-3-phenyl-2H-azirine (14491-02-2) → methyl (SR)-2-((RS)-3,3-dimethyl-2-phenylaziridin-2-yl)-3-oxo-2,3-dihydrobenzofuran-2-carboxylate

Guidance literature:

With bis(hexafluoroacetylacetonazo)nickel(II); In methanol; at 65 ℃; for 0.833333h;

DOI:10.1002/adsc.201900366

Reference yield: 66.0%

methyl 3-hydroxybenzofuran-2-carboxylate (5117-55-5) + 3-(2-nitrophenyl)-2H-azirine → methyl 2-[2-(2-nitrophenyl)aziridin-2-yl]-3-oxo-2,3-dihydrobenzofuran-2-carboxylate + methyl 2-[2-(2-nitrophenyl)aziridin-2-yl]-3-oxo-2,3-dihydrobenzofuran-2-carboxylate

Guidance literature:

With bis(hexafluoroacetylacetonazo)nickel(II); In methanol; at 65 ℃; for 0.116667h; Overall yield = 91 %; Overall yield = 61 mg;

DOI:10.1002/adsc.201900366

upstream raw materials:

methyl <(2-methoxycarbonyl)phenoxy>acetate

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