N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide

Base Information

• Chemical Name: N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide
• CAS No.: 174752-85-3
• Molecular Formula: C₁₀H₁₃ClN₄O
• Molecular Weight: 240.692
• Mol file: 174752-85-3.mol

Synonyms:174752-85-3;N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide;2-chloro-N-[3-(dimethylaminodiazenyl)phenyl]acetamide;2-Chloro-N-(3-(3,3-dimethyl-1-triazenyl)phenyl)acetamide;Acetamide, 2-chloro-N-(3-(3,3-dimethyl-1-triazenyl)phenyl)-;2-CHLORO-N-(3-DIMETHYLAMINODIAZENYLPHENYL)ACETAMIDE;C10H13ClN4O;2-Chloro-N-{3-[(1E)-3,3-dimethyl-1-triazen-1-yl]phenyl}acetamide;LS-8513;C10-H13-Cl-N4-O;ZKJZJYISLSSXLK-UHFFFAOYSA-N

Chemical Property of N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 60.55000
• Density: 1.23g/cm³
• LogP: 3.07370
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 240.0777887
• Heavy Atom Count: 16
• Complexity: 257

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)N=NC1=CC=CC(=C1)NC(=O)CCl

Technology Process of N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide

There total 2 articles about N-(3-(3,3-Dimethyltriazeno)phenyl)chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

dimethyl amine (124-40-3) + 3-(2-chloro-acetylamino)-benzenediazonium; chloride → N-[3-(3,3-dimethyltriazeno)phenyl]chloroacetamide (174752-85-3)

Guidance literature:

potassium hydroxide; sodium acetate; In water; at -5 - -2 ℃; for 3h;

DOI:10.1007/BF02218920

Reference yield:

2-chloro-5-amino-acetanilide → N-[3-(3,3-dimethyltriazeno)phenyl]chloroacetamide (174752-85-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaNO₂ / aq. HCl / H₂O / 0.5 h / -2 - 0 °C

2: 56 percent / KOH; sodium acetate / H₂O / 3 h / -5 - -2 °C

With sodium nitrite; hydrogenchloride; potassium hydroxide; sodium acetate; In water; 1: Diazotization / 2: azocombination;

DOI:10.1007/BF02218920

upstream raw materials:

dimethyl amine

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