2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane

Base Information

Chemical Name:2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane
CAS No.:7241-35-2
Molecular Formula:C₂₀H₃₂O₂
Molecular Weight:304.473
Hs Code.:
DSSTox Substance ID:DTXSID00413792

Synonyms:7241-35-2;2,8-bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane;DTXSID00413792

Suppliers and Price of 2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane

Chemical Property:

Vapor Pressure:1.06E-05mmHg at 25°C
Boiling Point:382.2°C at 760 mmHg
Flash Point:156.9°C
Density:1.59g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:341.96531
Heavy Atom Count:15
Complexity:189

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(OC2(C1)CCCC(O2)CBr)CBr

Technology Process of 2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane

There total 34 articles about 2,8-Bis(bromomethyl)-1,7-dioxaspiro[5.5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 641-82-7,641-84-9,4085-03-4,63088-07-3,63121-01-7,88729-24-2,88729-25-3,88729-26-4,88729-27-5,88980-24-9,103881-21-6,120925-80-6,641-83-8
ZIN⁽²²³⁾C₀₅₄₅₁

: 521-11-9,7241-35-2
mestanolone

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 65 ℃; for 2h;
DOI:10.1248/cpb.52.989

Reference yield: 82.8%

: C₂₂H₃₆O₂

: 521-11-9,7241-35-2
mestanolone

Guidance literature:: With toluene-4-sulfonic acid; In chloroform; at 50 - 55 ℃; Reagent/catalyst; Solvent;

Reference yield:

: 74-87-3
methylene chloride

: 972-46-3
3-ethoxyandrosta-3,5-dien-17-one

: 521-11-9,7241-35-2
mestanolone

Guidance literature:: methylene chloride; With iodine; magnesium; In tetrahydrofuran; at 40 - 45 ℃; for 1h;

3-ethoxyandrosta-3,5-dien-17-one; In tetrahydrofuran; at 10 - 45 ℃; for 12.08h; Further stages;